phenyl 2-(N-acetylamino)-3,4,6-tri-O-acetyl-2-deoxy-1-seleno-β-D-glucopyranoside

Base Information

Chemical Name:phenyl 2-(N-acetylamino)-3,4,6-tri-O-acetyl-2-deoxy-1-seleno-β-D-glucopyranoside
CAS No.:275370-61-1
Molecular Formula:C₂₀H₂₅NO₈Se
Molecular Weight:486.38
Hs Code.:

Synonyms:phenyl 2-(N-acetylamino)-3,4,6-tri-O-acetyl-2-deoxy-1-seleno-β-D-glucopyranoside

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Chemical Property of phenyl 2-(N-acetylamino)-3,4,6-tri-O-acetyl-2-deoxy-1-seleno-β-D-glucopyranoside

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Technology Process of phenyl 2-(N-acetylamino)-3,4,6-tri-O-acetyl-2-deoxy-1-seleno-β-D-glucopyranoside

There total 4 articles about phenyl 2-(N-acetylamino)-3,4,6-tri-O-acetyl-2-deoxy-1-seleno-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 33861-17-5
phenyl trimethylsilyl selenide

: 3006-60-8,4539-83-7,6730-10-5,7772-79-4,7784-54-5,10385-50-9,14086-90-9,26151-16-6,76375-60-5,76375-61-6,95341-98-3,95341-99-4,134451-91-5,134451-96-0,136982-81-5,145375-11-7,148347-15-3
2-acetamido-1,3,4,6-tetra-O-acetyl-2-deoxy-β-D-glucopyranose

: 275370-61-1
phenyl 2-(N-acetylamino)-3,4,6-tri-O-acetyl-2-deoxy-1-seleno-β-D-glucopyranoside

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In 1,2-dichloro-ethane; at 50 ℃; for 48h;
DOI:10.1021/ol0269695

Reference yield: 82.0%

: 645-96-5
Benzeneselenol

: 10378-06-0,20757-53-3,35954-65-5,123483-77-2,134308-33-1
2-methyl-(3,4,6-tri-O-acetyl-1,2-dideoxy-α-D-glucopyranoso)[1,2-d]-2-oxazoline

: 275370-61-1
phenyl 2-(N-acetylamino)-3,4,6-tri-O-acetyl-2-deoxy-1-seleno-β-D-glucopyranoside

Guidance literature:: With camphor-10-sulfonic acid; In 1,2-dichloro-ethane; for 3h; Heating;
DOI:10.1021/ol0269695

Reference yield: 79.0%

: 1666-13-3
diphenyl diselenide

: 3068-34-6
Acetic acid (2R,3S,4R,5R,6R)-3-acetoxy-2-acetoxymethyl-5-acetylamino-6-chloro-tetrahydro-pyran-4-yl ester

: 275370-61-1
phenyl 2-(N-acetylamino)-3,4,6-tri-O-acetyl-2-deoxy-1-seleno-β-D-glucopyranoside

Guidance literature:: diphenyl diselenide; With rongalite; potassium carbonate; In N,N-dimethyl-formamide; at 25 ℃; for 0.166667h;

Acetic acid (2R,3S,4R,5R,6R)-3-acetoxy-2-acetoxymethyl-5-acetylamino-6-chloro-tetrahydro-pyran-4-yl ester; In N,N-dimethyl-formamide; at 25 ℃; for 2h;
DOI:10.1016/j.carres.2014.07.011