methyl 1-{3-[(3-chloro-1,4-dioxo-1,4-dihydro-2-naphthalenyl)oxy]phenyl}-5-oxo-3-pyrrolidinecarboxylate

Base Information

Chemical Name:methyl 1-{3-[(3-chloro-1,4-dioxo-1,4-dihydro-2-naphthalenyl)oxy]phenyl}-5-oxo-3-pyrrolidinecarboxylate
CAS No.:1427549-79-8
Molecular Formula:C₂₂H₁₆ClNO₆
Molecular Weight:425.825
Hs Code.:

Synonyms:methyl 1-{3-[(3-chloro-1,4-dioxo-1,4-dihydro-2-naphthalenyl)oxy]phenyl}-5-oxo-3-pyrrolidinecarboxylate

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Chemical Property of methyl 1-{3-[(3-chloro-1,4-dioxo-1,4-dihydro-2-naphthalenyl)oxy]phenyl}-5-oxo-3-pyrrolidinecarboxylate

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Technology Process of methyl 1-{3-[(3-chloro-1,4-dioxo-1,4-dihydro-2-naphthalenyl)oxy]phenyl}-5-oxo-3-pyrrolidinecarboxylate

There total 2 articles about methyl 1-{3-[(3-chloro-1,4-dioxo-1,4-dihydro-2-naphthalenyl)oxy]phenyl}-5-oxo-3-pyrrolidinecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 117-80-6
2,3-Dichloro-1,4-naphthoquinone

: 101626-19-1
N-(3-hydroxyphenyl)-2-oxopyrrolidine-4-carboxylic acid methyl ester

: 1427549-79-8
methyl 1-{3-[(3-chloro-1,4-dioxo-1,4-dihydro-2-naphthalenyl)oxy]phenyl}-5-oxo-3-pyrrolidinecarboxylate

Guidance literature:: With sodium carbonate; In dimethyl sulfoxide; at 20 ℃; for 24h;
DOI:10.3390/molecules171214434

Reference yield:

: 91891-24-6
N-(3-hydroxyphenyl)-2-oxopyrrolidine-4-carboxylic acid

: 1427549-79-8
methyl 1-{3-[(3-chloro-1,4-dioxo-1,4-dihydro-2-naphthalenyl)oxy]phenyl}-5-oxo-3-pyrrolidinecarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: sulfuric acid / 5 h / Reflux

2: sodium carbonate / dimethyl sulfoxide / 24 h / 20 °C

With sulfuric acid; sodium carbonate; In dimethyl sulfoxide;
DOI:10.3390/molecules171214434