2,3,4-tri-O-benzoyl-α-D-mannopyranosyl-(1->6)-2,3,4-tri-O-benzoyl-α-D-mannopyranosyl fluoride

Base Information

• Chemical Name: 2,3,4-tri-O-benzoyl-α-D-mannopyranosyl-(1->6)-2,3,4-tri-O-benzoyl-α-D-mannopyranosyl fluoride
• CAS No.: 1178514-93-6
• Molecular Formula: C₅₄H₄₅FO₁₆
• Molecular Weight: 968.94

Synonyms:2,3,4-tri-O-benzoyl-α-D-mannopyranosyl-(1->6)-2,3,4-tri-O-benzoyl-α-D-mannopyranosyl fluoride

Chemical Property of 2,3,4-tri-O-benzoyl-α-D-mannopyranosyl-(1->6)-2,3,4-tri-O-benzoyl-α-D-mannopyranosyl fluoride

Chemical Property:

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Technology Process of 2,3,4-tri-O-benzoyl-α-D-mannopyranosyl-(1->6)-2,3,4-tri-O-benzoyl-α-D-mannopyranosyl fluoride

There total 1 articles about 2,3,4-tri-O-benzoyl-α-D-mannopyranosyl-(1->6)-2,3,4-tri-O-benzoyl-α-D-mannopyranosyl fluoride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

[(6-O-(1-methyl-3-imidazolio)acetyl)-2,3,4-tri-O-benzoyl-α-D-mannopyranosyl-(1->6)-2,3,4-tri-O-benzoyl-α-D-mannopyranosyl fluoride] hexafluorophosphate → 2,3,4-tri-O-benzoyl-α-D-mannopyranosyl-(1->6)-2,3,4-tri-O-benzoyl-α-D-mannopyranosyl fluoride (1178514-93-6)

Guidance literature:

With water; tetra-(n-butyl)ammonium iodide; sodium hydrogencarbonate; In diethyl ether; at 20 ℃;

DOI:10.1021/jo901169u

Reference yield: 82.0%

C67H59N2O17S(1+)*F6P(1-) (1005398-19-5) + 2,3,4-tri-O-benzoyl-α-D-mannopyranosyl-(1->6)-2,3,4-tri-O-benzoyl-α-D-mannopyranosyl fluoride (1178514-93-6) → [(6-O-(1-methyl-3-imidazolio)acetyl)-2,3,4-tri-O-benzoyl-α-D-mannopyranosyl-(1->6)-2,3,4-tri-O-benzoyl-α-D-mannopyranosyl-(1->6)-2,3,4-tri-O-benzoyl-α-D-mannopyranosyl-1-thio-2,3,4-tri-O-benzoyl-α-D-mannopyranosyl fluoride] hexafluorophosphate

Guidance literature:

With N-iodo-succinimide; trifluorormethanesulfonic acid; In dichloromethane; at -20 ℃; Inert atmosphere; Molecular sieve;

DOI:10.1021/jo901169u

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