1,3-bis(2,6-dimethyl-4-(morpholinomethyl)phenyl)-4,5-dihydro-1H-imidazol-3-ium-chloride

Base Information

Chemical Name:1,3-bis(2,6-dimethyl-4-(morpholinomethyl)phenyl)-4,5-dihydro-1H-imidazol-3-ium-chloride
CAS No.:1129711-28-9
Molecular Formula:C₂₉H₄₁N₄O₂*Cl
Molecular Weight:513.123
Hs Code.:

Synonyms:1,3-bis(2,6-dimethyl-4-(morpholinomethyl)phenyl)-4,5-dihydro-1H-imidazol-3-ium-chloride

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Chemical Property of 1,3-bis(2,6-dimethyl-4-(morpholinomethyl)phenyl)-4,5-dihydro-1H-imidazol-3-ium-chloride

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Technology Process of 1,3-bis(2,6-dimethyl-4-(morpholinomethyl)phenyl)-4,5-dihydro-1H-imidazol-3-ium-chloride

There total 2 articles about 1,3-bis(2,6-dimethyl-4-(morpholinomethyl)phenyl)-4,5-dihydro-1H-imidazol-3-ium-chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 1129711-22-3
N¹,N²-bis(2,6-dimethyl-4-(morpholinomethyl)phenyl)ethane-1,2-diamine

: 122-51-0
orthoformic acid triethyl ester

: 1129711-28-9
1,3-bis(2,6-dimethyl-4-(morpholinomethyl)phenyl)-4,5-dihydro-1H-imidazol-3-ium-chloride

Guidance literature:: With ammonium chloride; at 120 ℃; for 24h;
DOI:10.1039/b820633c

Reference yield:

: 74266-64-1
N-(amino-4, dimethyl-3,5)benzylmorpholine

: 1129711-28-9
1,3-bis(2,6-dimethyl-4-(morpholinomethyl)phenyl)-4,5-dihydro-1H-imidazol-3-ium-chloride

Guidance literature:: Multi-step reaction with 3 steps

1: formic acid / water; methanol / 192 h / 20 °C / Inert atmosphere

2: lithium aluminium tetrahydride / tetrahydrofuran / 30.25 h / 0 - 20 °C

3: ammonium chloride / 2.5 h / 120 °C

With lithium aluminium tetrahydride; formic acid; ammonium chloride; In tetrahydrofuran; methanol; water;
DOI:10.1002/chem.201903155

Reference yield: 52.0%

: 1129711-28-9
1,3-bis(2,6-dimethyl-4-(morpholinomethyl)phenyl)-4,5-dihydro-1H-imidazol-3-ium-chloride

: 1129711-34-7
1,3-bis(2,6-dimethyl-4-(chloromethyl)phenyl)-4,5-dihydro-1H-imidazol-3-ium-chloride

Guidance literature:: 1,3-bis(2,6-dimethyl-4-(morpholinomethyl)phenyl)-4,5-dihydro-1H-imidazol-3-ium-chloride; With chloroformic acid ethyl ester; In acetonitrile; for 8h; Reflux;

With chloroformic acid ethyl ester; In acetonitrile; for 8h; Reflux;
DOI:10.1039/b820633c