benzyl(cyclohexa-1,4-dien-3-yl)phosphinic acid N,N-diethylamide

Base Information

Chemical Name:benzyl(cyclohexa-1,4-dien-3-yl)phosphinic acid N,N-diethylamide
CAS No.:1449303-45-0
Molecular Formula:C₁₇H₂₄NOP
Molecular Weight:289.357
Hs Code.:

Synonyms:benzyl(cyclohexa-1,4-dien-3-yl)phosphinic acid N,N-diethylamide

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Chemical Property of benzyl(cyclohexa-1,4-dien-3-yl)phosphinic acid N,N-diethylamide

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Technology Process of benzyl(cyclohexa-1,4-dien-3-yl)phosphinic acid N,N-diethylamide

There total 4 articles about benzyl(cyclohexa-1,4-dien-3-yl)phosphinic acid N,N-diethylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 1449303-16-5
benzylphenylphosphinic acid N,N-diethylamide

: 1449303-45-0
benzyl(cyclohexa-1,4-dien-3-yl)phosphinic acid N,N-diethylamide

Guidance literature:: With ammonia; sodium; In tetrahydrofuran; at -78 ℃; for 0.0833333h; Inert atmosphere; Schlenk technique;
DOI:10.1002/ejoc.201300344

Reference yield:

: 20335-99-3,20428-90-4,177334-60-0
benzyl (phenyl)phosphine oxide

: 1449303-45-0
benzyl(cyclohexa-1,4-dien-3-yl)phosphinic acid N,N-diethylamide

Guidance literature:: Multi-step reaction with 4 steps

1: phosphorus trichloride / dichloromethane / 1.5 h / 20 °C / Inert atmosphere; Schlenk technique

2: dichloromethane / 2 h / 20 °C / Inert atmosphere; Schlenk technique

3: dihydrogen peroxide / dichloromethane / 20 °C / Inert atmosphere; Schlenk technique

4: ammonia; sodium / tetrahydrofuran / 0.08 h / -78 °C / Inert atmosphere; Schlenk technique

With ammonia; dihydrogen peroxide; sodium; phosphorus trichloride; In tetrahydrofuran; dichloromethane; 4: |Birch Reduction;
DOI:10.1002/ejoc.201300344

Reference yield:

: 29949-68-6,73365-16-9
benzyl-phenylchlorophosphine

: 1449303-45-0
benzyl(cyclohexa-1,4-dien-3-yl)phosphinic acid N,N-diethylamide

Guidance literature:: Multi-step reaction with 3 steps

1: dichloromethane / 2 h / 20 °C / Inert atmosphere; Schlenk technique

2: dihydrogen peroxide / dichloromethane / 20 °C / Inert atmosphere; Schlenk technique

3: ammonia; sodium / tetrahydrofuran / 0.08 h / -78 °C / Inert atmosphere; Schlenk technique

With ammonia; dihydrogen peroxide; sodium; In tetrahydrofuran; dichloromethane; 3: |Birch Reduction;
DOI:10.1002/ejoc.201300344