{(E)-Amino[(2Z)-{[4-(dimethylamino)phenyl]methylidene}hydrazinylidene]methyl}selanyl

Base Information

Chemical Name:{(E)-Amino[(2Z)-{[4-(dimethylamino)phenyl]methylidene}hydrazinylidene]methyl}selanyl
CAS No.:58531-92-3
Molecular Formula:C₁₀H₁₄N₄Se
Molecular Weight:269.208
Hs Code.:
NSC Number:156128
DSSTox Substance ID:DTXSID00423018

Synonyms:58531-92-3;DTXSID00423018;NSC156128;NSC-156128;{(E)-Amino[(2Z)-{[4-(dimethylamino)phenyl]methylidene}hydrazinylidene]methyl}selanyl

Suppliers and Price of {(E)-Amino[(2Z)-{[4-(dimethylamino)phenyl]methylidene}hydrazinylidene]methyl}selanyl

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of {(E)-Amino[(2Z)-{[4-(dimethylamino)phenyl]methylidene}hydrazinylidene]methyl}selanyl

Chemical Property:

Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:269.03054
Heavy Atom Count:15
Complexity:242

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CN(C)C1=CC=C(C=C1)C=NN=C(N)[Se]
Isomeric SMILES:CN(C)C1=CC=C(C=C1)/C=N\N=C(/N)\[Se]

Technology Process of {(E)-Amino[(2Z)-{[4-(dimethylamino)phenyl]methylidene}hydrazinylidene]methyl}selanyl

There total 3 articles about {(E)-Amino[(2Z)-{[4-(dimethylamino)phenyl]methylidene}hydrazinylidene]methyl}selanyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 5.0%

: 2929-82-0
4-dimethylamino-benzaldehyde semicarbazone

: 58531-92-3
p-dimethylaminobenzaldehyde selenosemicarbazone

Guidance literature:: 4-dimethylamino-benzaldehyde semicarbazone; With phosphorus pentachloride; In dichloromethane; at 0 - 20 ℃; for 0.5h;

With lithium aluminum hydride hydroselenide; In tetrahydrofuran; dichloromethane; at 0 ℃; for 1h;

Reference yield:

: 100-10-7
4-dimethylamino-benzaldehyde

: 21198-80-1
acetone selenosemicarbazone

: 58531-92-3
p-dimethylaminobenzaldehyde selenosemicarbazone

Guidance literature:: DOI:10.1111/j.1540-8191.2001.tb00551.x

Reference yield:

: 100-10-7
4-dimethylamino-benzaldehyde

: 58531-92-3
p-dimethylaminobenzaldehyde selenosemicarbazone

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium acetate / ethanol / 0.25 h / 20 °C

1.2: 20 °C

2.1: phosphorus pentachloride / dichloromethane / 0.5 h / 0 - 20 °C

2.2: 1 h / 0 °C

With phosphorus pentachloride; sodium acetate; In ethanol; dichloromethane;