C₂₆H₂₇N₅O

Base Information

Chemical Name:C₂₆H₂₇N₅O
CAS No.:1346245-24-6
Molecular Formula:C₂₆H₂₇N₅O
Molecular Weight:425.533
Hs Code.:

C<sub>26</sub>H<sub>27</sub>N<sub>5</sub>O

Synonyms:C₂₆H₂₇N₅O

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Chemical Property of C₂₆H₂₇N₅O

Chemical Property:

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Technology Process of C₂₆H₂₇N₅O

There total 6 articles about C₂₆H₂₇N₅O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 1346245-23-5
N-phenyl-3-(1-(tetrahydro-2H-pyran-2-yl)-1H-pyrazol-4-yl)quinoxaline-6-amine

: 7051-34-5
cyclopropylcarbinyl bromide

: 1346245-24-6
C₂₆H₂₇N₅O

Guidance literature:: N-phenyl-3-(1-(tetrahydro-2H-pyran-2-yl)-1H-pyrazol-4-yl)quinoxaline-6-amine; With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 5 ℃; for 0.5h;

cyclopropylcarbinyl bromide; In N,N-dimethyl-formamide; mineral oil; at 5 - 20 ℃;

Reference yield:

: 110-87-2
3,4-dihydro-2H-pyran

: 1346245-24-6
C₂₆H₂₇N₅O

Guidance literature:: Multi-step reaction with 3 steps

1.1: trifluoroacetic acid / toluene / 48 h / 60 °C

2.1: sodium t-butanolate / palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl / 1,2-dimethoxyethane / 4 h / Inert atmosphere; Reflux

3.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.5 h / 5 °C

3.2: 5 - 20 °C

With sodium hydride; sodium t-butanolate; palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; trifluoroacetic acid; In 1,2-dimethoxyethane; N,N-dimethyl-formamide; toluene; mineral oil;

Reference yield:

: 82031-32-1
7-bromo-1H-quinoxalin-2-one

: 1346245-24-6
C₂₆H₂₇N₅O

Guidance literature:: Multi-step reaction with 4 steps

1.1: trichlorophosphate / 2 h / 100 °C

1.2: Cooling with ice

2.1: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,2-dimethoxyethane / 20 h / Inert atmosphere; Reflux

3.1: sodium t-butanolate / palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl / 1,2-dimethoxyethane / 4 h / Inert atmosphere; Reflux

4.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.5 h / 5 °C

4.2: 5 - 20 °C

With sodium hydride; sodium carbonate; sodium t-butanolate; trichlorophosphate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; In 1,2-dimethoxyethane; N,N-dimethyl-formamide; mineral oil;