p-methoxyphenyl 4,6-O-p-methoxyphenylbenzylidene-3-deoxy-3-C-(difluoromethylene)-β-D-xylo-hex-3-ulopyranoside

Base Information

• Chemical Name: p-methoxyphenyl 4,6-O-p-methoxyphenylbenzylidene-3-deoxy-3-C-(difluoromethylene)-β-D-xylo-hex-3-ulopyranoside
• CAS No.: 1001847-02-4
• Molecular Formula: C₂₂H₂₂F₂O₇
• Molecular Weight: 436.409

Synonyms:p-methoxyphenyl 4,6-O-p-methoxyphenylbenzylidene-3-deoxy-3-C-(difluoromethylene)-β-D-xylo-hex-3-ulopyranoside

Chemical Property of p-methoxyphenyl 4,6-O-p-methoxyphenylbenzylidene-3-deoxy-3-C-(difluoromethylene)-β-D-xylo-hex-3-ulopyranoside

Chemical Property:

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Technology Process of p-methoxyphenyl 4,6-O-p-methoxyphenylbenzylidene-3-deoxy-3-C-(difluoromethylene)-β-D-xylo-hex-3-ulopyranoside

There total 1 articles about p-methoxyphenyl 4,6-O-p-methoxyphenylbenzylidene-3-deoxy-3-C-(difluoromethylene)-β-D-xylo-hex-3-ulopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C31H42F2O7Si (1001847-18-2) → p-methoxyphenyl 4,6-O-p-methoxyphenylbenzylidene-3-deoxy-3-C-(difluoromethylene)-β-D-xylo-hex-3-ulopyranoside (1001847-02-4)

Guidance literature:

With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 0 ℃; for 0.0833333h;

DOI:10.1021/ja075738w

Reference yield: 72.0%

p-methoxyphenyl 4,6-O-p-methoxyphenylbenzylidene-3-deoxy-3-C-(difluoromethylene)-β-D-xylo-hex-3-ulopyranoside (1001847-02-4) + N-acetyl-4,7,8,9-tetra-O-benzyloxymethyl-2-deoxy-neuraminic acid (1001846-99-6) → C65H71F2NO18 (1001847-03-5)

Guidance literature:

With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃; for 5h;

DOI:10.1021/ja075738w

upstream raw materials:

C₃₁H₄₂F₂O₇Si

Downstream raw materials:

C₆₅H₇₁F₂NO₁₈

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