3-benzyl-<3,4-di-O-benzyl-1,2-dideoxy-α-D-glucopyrano>-<2,1-d>-2-oxazolidone

Base Information

Chemical Name:3-benzyl-<3,4-di-O-benzyl-1,2-dideoxy-α-D-glucopyrano>-<2,1-d>-2-oxazolidone
CAS No.:142269-97-4
Molecular Formula:C₂₈H₂₉NO₆
Molecular Weight:475.541
Hs Code.:

Synonyms:3-benzyl-<3,4-di-O-benzyl-1,2-dideoxy-α-D-glucopyrano>-<2,1-d>-2-oxazolidone

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Chemical Property of 3-benzyl-<3,4-di-O-benzyl-1,2-dideoxy-α-D-glucopyrano>-<2,1-d>-2-oxazolidone

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Technology Process of 3-benzyl-<3,4-di-O-benzyl-1,2-dideoxy-α-D-glucopyrano>-<2,1-d>-2-oxazolidone

There total 3 articles about 3-benzyl-<3,4-di-O-benzyl-1,2-dideoxy-α-D-glucopyrano>-<2,1-d>-2-oxazolidone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 142269-91-8
2-allyloxycarbonylamino-1,6-anhydro-2-N-benzyl-3,4-di-O-benzyl-2-deoxy-β-D-glucopyranose

: 142269-97-4
3-benzyl-<3,4-di-O-benzyl-1,2-dideoxy-α-D-glucopyrano>-<2,1-d>-2-oxazolidone

Guidance literature:: With titanium tetrachloride; In dichloromethane; for 16h; Ambient temperature;
DOI:10.1016/S0008-6215(00)90550-0

Reference yield:

: 100-44-7
benzyl chloride

: 142269-97-4
3-benzyl-<3,4-di-O-benzyl-1,2-dideoxy-α-D-glucopyrano>-<2,1-d>-2-oxazolidone

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / NaH, tetrabutylammonium iodide / tetrahydrofuran / 1 h / Ambient temperature

2: 82 percent / TiCl₄ / CH₂Cl₂ / 16 h / Ambient temperature

With titanium tetrachloride; tetra-(n-butyl)ammonium iodide; sodium hydride; In tetrahydrofuran; dichloromethane;
DOI:10.1016/S0008-6215(00)90550-0

Reference yield:

: 121363-69-7
2-N-Allyloxycarbonyl-2-amino-1,6-anhydro-2-deoxy-β-D-glucopyranose

: 142269-97-4
3-benzyl-<3,4-di-O-benzyl-1,2-dideoxy-α-D-glucopyrano>-<2,1-d>-2-oxazolidone

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / NaH, tetrabutylammonium iodide / tetrahydrofuran / 1 h / Ambient temperature

2: 82 percent / TiCl₄ / CH₂Cl₂ / 16 h / Ambient temperature

With titanium tetrachloride; tetra-(n-butyl)ammonium iodide; sodium hydride; In tetrahydrofuran; dichloromethane;
DOI:10.1016/S0008-6215(00)90550-0