7-[2-fluoro-4-(methylsulfonyl)phenyl]-4-(4-piperidinyloxy)-6,7-dihydro-5H-pyrrolo[2,3-d]pyrimidine trifluoroacetate

Base Information

Chemical Name:7-[2-fluoro-4-(methylsulfonyl)phenyl]-4-(4-piperidinyloxy)-6,7-dihydro-5H-pyrrolo[2,3-d]pyrimidine trifluoroacetate
CAS No.:1001398-45-3
Molecular Formula:C₂HF₃O₂*C₁₈H₂₁FN₄O₃S
Molecular Weight:506.478
Hs Code.:

Synonyms:7-[2-fluoro-4-(methylsulfonyl)phenyl]-4-(4-piperidinyloxy)-6,7-dihydro-5H-pyrrolo[2,3-d]pyrimidine trifluoroacetate

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Chemical Property of 7-[2-fluoro-4-(methylsulfonyl)phenyl]-4-(4-piperidinyloxy)-6,7-dihydro-5H-pyrrolo[2,3-d]pyrimidine trifluoroacetate

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Technology Process of 7-[2-fluoro-4-(methylsulfonyl)phenyl]-4-(4-piperidinyloxy)-6,7-dihydro-5H-pyrrolo[2,3-d]pyrimidine trifluoroacetate

There total 1 articles about 7-[2-fluoro-4-(methylsulfonyl)phenyl]-4-(4-piperidinyloxy)-6,7-dihydro-5H-pyrrolo[2,3-d]pyrimidine trifluoroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1001397-21-2
1,1-dimethylethyl 4-({7-[2-fluoro-4-(methylsulfonyl)phenyl]-6,7-dihydro-5H-pyrrolo[2,3-d]pyrimidin-4-yl}oxy)-1-piperidinecarboxylate

: 76-05-1
trifluoroacetic acid

: 1001398-45-3
7-[2-fluoro-4-(methylsulfonyl)phenyl]-4-(4-piperidinyloxy)-6,7-dihydro-5H-pyrrolo[2,3-d]pyrimidine trifluoroacetate

Guidance literature:: In dichloromethane; at 20 ℃; for 1 - 2h; Product distribution / selectivity;

Reference yield: 70.0%

: 1001398-45-3
7-[2-fluoro-4-(methylsulfonyl)phenyl]-4-(4-piperidinyloxy)-6,7-dihydro-5H-pyrrolo[2,3-d]pyrimidine trifluoroacetate

: 594-44-5
Ethanesulfonyl chloride

: 1001398-90-8
4-{[1-(ethylsulfonyl)-4-piperidinyl]oxy}-7-[2-fluoro-4-(methylsulfonyl)phenyl]-6,7-dihydro-5H-pyrrolo[2,3-d]pyrimidine

Guidance literature:: 7-[2-fluoro-4-(methylsulfonyl)phenyl]-4-(4-piperidinyloxy)-6,7-dihydro-5H-pyrrolo[2,3-d]pyrimidine trifluoroacetate; With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 0.5h;

Ethanesulfonyl chloride; In dichloromethane; at 20 ℃; for 18h;