C₄₁H₄₈O₁₁

Base Information

• Chemical Name: C₄₁H₄₈O₁₁
• CAS No.: 1313741-18-2
• Molecular Formula: C₄₁H₄₈O₁₁
• Molecular Weight: 716.826
• Mol file: 1313741-18-2.mol

Synonyms:C₄₁H₄₈O₁₁

Chemical Property of C₄₁H₄₈O₁₁

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₄₁H₄₈O₁₁

There total 3 articles about C₄₁H₄₈O₁₁ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3,4,5,7-tetra-O-benzyl-1-deoxy-α-D-gluco-hept-2-ulopyranosyl-(2→1)-2,3,4,6-tetra-O-acetyl-α-D-glucopyranoside (1274877-45-0) → C41H48O11 (1313741-18-2)

Guidance literature:

3,4,5,7-tetra-O-benzyl-1-deoxy-α-D-gluco-hept-2-ulopyranosyl-(2→1)-2,3,4,6-tetra-O-acetyl-α-D-glucopyranoside; With methanol; sodium methylate; at 20 ℃; for 1h;

In methanol;

Reference yield:

2,3,4,5-tetra-O-acetyl-D-glucopyranose (3947-62-4,6207-76-7,19235-21-3,22554-70-7,22860-22-6,47339-09-3,57884-82-9,62057-79-8,70191-05-8,109525-54-4,140147-37-1,10343-06-3) → C41H48O11 (1313741-18-2)

Guidance literature:

Multi-step reaction with 2 steps

1.1: trimethylsilyl trifluoromethanesulfonate / dichloromethane / 3 h / -40 °C / Molecular sieve; Inert atmosphere

2.1: sodium methylate; methanol / 1 h / 20 °C

2.2: DOWEX 50WX₈ (H⁺ form) ion exchange resin

With methanol; sodium methylate; trimethylsilyl trifluoromethanesulfonate; In dichloromethane;

Reference yield:

3,4,5,7-tetra-O-benzyl-1-deoxy-α-D-gluco-hept-2-ulopyranose (137344-41-3) → C41H48O11 (1313741-18-2)

Guidance literature:

Multi-step reaction with 2 steps

1.1: trimethylsilyl trifluoromethanesulfonate / dichloromethane / 3 h / -40 °C / Molecular sieve; Inert atmosphere

2.1: sodium methylate; methanol / 1 h / 20 °C

2.2: DOWEX 50WX₈ (H⁺ form) ion exchange resin

With methanol; sodium methylate; trimethylsilyl trifluoromethanesulfonate; In dichloromethane;

upstream raw materials:

2,3,4,5-tetra-O-acetyl-D-glucopyranose

3,4,5,7-tetra-O-benzyl-1-deoxy-α-D-gluco-hept-2-ulopyranose

3,4,5,7-tetra-O-benzyl-1-deoxy-α-D-gluco-hept-2-ulopyranosyl-(2→1)-2,3,4,6-tetra-O-acetyl-α-D-glucopyranoside