N-(9-fluorenylmethoxycarbonyl)-O-[(methyl 2,3,4-tri-O-acetyl-β-D-glucopyranosyluronate)-(1->3)-O-(2,4,6-tri-O-acetyl-β-D-galactopyranosyl)-(1->3)-O-(2,4,6-tri-O-acetyl-β-D-galactopyranosyl)-(1->4)-2,3-di-O-(4-methylbenzoyl)-β-D-xylopyranosyl]-L-serylglycine allyl ester

Base Information

Chemical Name:N-(9-fluorenylmethoxycarbonyl)-O-[(methyl 2,3,4-tri-O-acetyl-β-D-glucopyranosyluronate)-(1->3)-O-(2,4,6-tri-O-acetyl-β-D-galactopyranosyl)-(1->3)-O-(2,4,6-tri-O-acetyl-β-D-galactopyranosyl)-(1->4)-2,3-di-O-(4-methylbenzoyl)-β-D-xylopyranosyl]-L-serylglycine allyl ester
CAS No.:1254303-64-4
Molecular Formula:C₈₁H₉₂N₂O₃₇
Molecular Weight:1685.61
Hs Code.:

N-(9-fluorenylmethoxycarbonyl)-O-[(methyl 2,3,4-tri-O-acetyl-β-D-glucopyranosyluronate)-(1->3)-O-(2,4,6-tri-O-acetyl-β-D-galactopyranosyl)-(1->3)-O-(2,4,6-tri-O-acetyl-β-D-galactopyranosyl)-(1->4)-2,3-di-O-(4-methylbenzoyl)-β-D-xylopyranosyl]-L-serylglycine allyl ester

Synonyms:N-(9-fluorenylmethoxycarbonyl)-O-[(methyl 2,3,4-tri-O-acetyl-β-D-glucopyranosyluronate)-(1->3)-O-(2,4,6-tri-O-acetyl-β-D-galactopyranosyl)-(1->3)-O-(2,4,6-tri-O-acetyl-β-D-galactopyranosyl)-(1->4)-2,3-di-O-(4-methylbenzoyl)-β-D-xylopyranosyl]-L-serylglycine allyl ester

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Chemical Property of N-(9-fluorenylmethoxycarbonyl)-O-[(methyl 2,3,4-tri-O-acetyl-β-D-glucopyranosyluronate)-(1->3)-O-(2,4,6-tri-O-acetyl-β-D-galactopyranosyl)-(1->3)-O-(2,4,6-tri-O-acetyl-β-D-galactopyranosyl)-(1->4)-2,3-di-O-(4-methylbenzoyl)-β-D-xylopyranosyl]-L-serylglycine allyl ester

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Technology Process of N-(9-fluorenylmethoxycarbonyl)-O-[(methyl 2,3,4-tri-O-acetyl-β-D-glucopyranosyluronate)-(1->3)-O-(2,4,6-tri-O-acetyl-β-D-galactopyranosyl)-(1->3)-O-(2,4,6-tri-O-acetyl-β-D-galactopyranosyl)-(1->4)-2,3-di-O-(4-methylbenzoyl)-β-D-xylopyranosyl]-L-serylglycine allyl ester

There total 1 articles about N-(9-fluorenylmethoxycarbonyl)-O-[(methyl 2,3,4-tri-O-acetyl-β-D-glucopyranosyluronate)-(1->3)-O-(2,4,6-tri-O-acetyl-β-D-galactopyranosyl)-(1->3)-O-(2,4,6-tri-O-acetyl-β-D-galactopyranosyl)-(1->4)-2,3-di-O-(4-methylbenzoyl)-β-D-xylopyranosyl]-L-serylglycine allyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1254303-63-3
O-(methyl 2,3,4-tri-O-acetyl-β-D-glucopyranosyluronate)-(1->3)-O-(2,4,6-tri-O-acetyl-β-D-galactopyranosyl)-(1->3)-O-(2,4,6-tri-O-acetyl-β-D-galactopyranosyl)-(1->4)-2,3-di-O-(4-methylbenzoyl)-α-D-xylopyranosyl trichloroacetimidate

: 138479-84-2
N-(9-Fluorenylmethoxycarbonyl)-L-seryl-glycine allyl ester

: 1254303-64-4
N-(9-fluorenylmethoxycarbonyl)-O-[(methyl 2,3,4-tri-O-acetyl-β-D-glucopyranosyluronate)-(1->3)-O-(2,4,6-tri-O-acetyl-β-D-galactopyranosyl)-(1->3)-O-(2,4,6-tri-O-acetyl-β-D-galactopyranosyl)-(1->4)-2,3-di-O-(4-methylbenzoyl)-β-D-xylopyranosyl]-L-serylglycine allyl ester

Guidance literature:: O-(methyl 2,3,4-tri-O-acetyl-β-D-glucopyranosyluronate)-(1->3)-O-(2,4,6-tri-O-acetyl-β-D-galactopyranosyl)-(1->3)-O-(2,4,6-tri-O-acetyl-β-D-galactopyranosyl)-(1->4)-2,3-di-O-(4-methylbenzoyl)-α-D-xylopyranosyl trichloroacetimidate; N-(9-Fluorenylmethoxycarbonyl)-L-seryl-glycine allyl ester; In dichloromethane; at 20 ℃; for 0.5h; Molecular sieve; Inert atmosphere;

With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -20 ℃; Molecular sieve; Inert atmosphere;
DOI:10.1016/j.carres.2010.06.019

Reference yield: 93.0%

: 1254303-64-4
N-(9-fluorenylmethoxycarbonyl)-O-[(methyl 2,3,4-tri-O-acetyl-β-D-glucopyranosyluronate)-(1->3)-O-(2,4,6-tri-O-acetyl-β-D-galactopyranosyl)-(1->3)-O-(2,4,6-tri-O-acetyl-β-D-galactopyranosyl)-(1->4)-2,3-di-O-(4-methylbenzoyl)-β-D-xylopyranosyl]-L-serylglycine allyl ester

: 1254303-65-5
N-(9-fluorenylmethoxycarbonyl)-O-[(methyl 2,3,4-tri-O-acetyl-β-D-glucopyranosyluronate)-(1->3)-O-(2,4,6-tri-O-acetyl-β-D-galactopyranosyl)-(1->3)-O-(2,4,6-tri-O-acetyl-β-D-galactopyranosyl)-(1->4)-2,3-di-O-(4-methylbenzoyl)-β-D-xylopyranosyl]-L-serylglycine

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; N-methylaniline; In tetrahydrofuran; for 2h; Inert atmosphere;
DOI:10.1016/j.carres.2010.06.019