diisopropoxyphosphinothionyl tert-butylamino disulfide

Base Information

• Chemical Name: diisopropoxyphosphinothionyl tert-butylamino disulfide
• CAS No.: 76276-34-1
• Molecular Formula: C₁₀H₂₄NO₂PS₃
• Molecular Weight: 317.478
• Mol file: 76276-34-1.mol

Synonyms:diisopropoxyphosphinothionyl tert-butylamino disulfide

Chemical Property of diisopropoxyphosphinothionyl tert-butylamino disulfide

Chemical Property:

Purity/Quality:

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Technology Process of diisopropoxyphosphinothionyl tert-butylamino disulfide

There total 2 articles about diisopropoxyphosphinothionyl tert-butylamino disulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.5%

diisopropoxyphosphinothionyl tert-butylamino trisulfide (76289-06-0) + triphenylphosphine (603-35-0) → diisopropoxyphosphinothionyl tert-butylamino disulfide (76276-34-1) + triphenylphosphine sulfide (3878-45-3)

Guidance literature:

In diethyl ether; at 0 ℃; for 0.25h;

Reference yield: 63.5%

diisopropoxyphosphinothionyl tert-butylamino trisulfide (76289-06-0) + triethyl phosphite (122-52-1) → O,O,O-triethyl phosphorothioate (126-68-1) + diisopropoxyphosphinothionyl tert-butylamino disulfide (76276-34-1)

Guidance literature:

In diethyl ether; at 0 ℃; for 0.25h;

upstream raw materials:

diisopropoxyphosphinothionyl tert-butylamino trisulfide

triphenylphosphine

triethyl phosphite

Refernces