2-Benzyl-1,2,3,5-tetrahydro-5,9b-o-benzenobenzisoindole

Base Information

Chemical Name:2-Benzyl-1,2,3,5-tetrahydro-5,9b-o-benzenobenzisoindole
CAS No.:56948-89-1
Molecular Formula:C₂₅H₂₁N
Molecular Weight:335.448
Hs Code.:

2-Benzyl-1,2,3,5-tetrahydro-5,9b-o-benzenobenz<e>isoindole

Synonyms:2-Benzyl-1,2,3,5-tetrahydro-5,9b-o-benzenobenzisoindole

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Chemical Property of 2-Benzyl-1,2,3,5-tetrahydro-5,9b-o-benzenobenzisoindole

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Technology Process of 2-Benzyl-1,2,3,5-tetrahydro-5,9b-o-benzenobenzisoindole

There total 5 articles about 2-Benzyl-1,2,3,5-tetrahydro-5,9b-o-benzenobenzisoindole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 57447-08-2
N-Benzyl-N-propargyl-9-anthracenemethanamine

: 56948-89-1
2-Benzyl-1,2,3,5-tetrahydro-5,9b-o-benzenobenzisoindole

Guidance literature:: In toluene; at 111 ℃; for 2.2h;
DOI:10.1021/jo01296a031

Reference yield:

: 57447-07-1
9-[(N-benzylamino)methyl]anthracene

: 56948-89-1
2-Benzyl-1,2,3,5-tetrahydro-5,9b-o-benzenobenzisoindole

Guidance literature:: Multi-step reaction with 2 steps

1: 15percent aq. sodium hydroxide / CH₂Cl₂ / 3 h / Ambient temperature

2: 76 percent / toluene / 2.2 h / 111 °C

With sodium hydroxide; In dichloromethane; toluene;
DOI:10.1021/jo01296a031

Reference yield:

: 14607-11-5
1-(anthracen-9-yl)-N-benzylmethanimine

: 56948-89-1
2-Benzyl-1,2,3,5-tetrahydro-5,9b-o-benzenobenzisoindole

Guidance literature:: Multi-step reaction with 3 steps

1: 139.9 g / Sodium borohydride / ethanol / 1.) 60-65 deg C, 2.) RT, overnight

2: 15percent aq. sodium hydroxide / CH₂Cl₂ / 3 h / Ambient temperature

3: 76 percent / toluene / 2.2 h / 111 °C

With sodium hydroxide; sodium tetrahydroborate; In ethanol; dichloromethane; toluene;
DOI:10.1021/jo01296a031