Benzyl-2-acetamido-3,6-di-O-benzyl-2-desoxy-4-O-(β-D-galactopyranosyl)-α-D-glucopyranosid

Base Information

Chemical Name:Benzyl-2-acetamido-3,6-di-O-benzyl-2-desoxy-4-O-(β-D-galactopyranosyl)-α-D-glucopyranosid
CAS No.:70209-54-0
Molecular Formula:C₃₅H₄₃NO₁₁
Molecular Weight:653.727
Hs Code.:

Synonyms:Benzyl-2-acetamido-3,6-di-O-benzyl-2-desoxy-4-O-(β-D-galactopyranosyl)-α-D-glucopyranosid

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Chemical Property of Benzyl-2-acetamido-3,6-di-O-benzyl-2-desoxy-4-O-(β-D-galactopyranosyl)-α-D-glucopyranosid

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Technology Process of Benzyl-2-acetamido-3,6-di-O-benzyl-2-desoxy-4-O-(β-D-galactopyranosyl)-α-D-glucopyranosid

There total 7 articles about Benzyl-2-acetamido-3,6-di-O-benzyl-2-desoxy-4-O-(β-D-galactopyranosyl)-α-D-glucopyranosid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 58700-48-4
Benzyl-2-acetamido-3,6-di-O-benzyl-2-desoxy-4-O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-α-D-glucopyranosid

: 70209-54-0
Benzyl-2-acetamido-3,6-di-O-benzyl-2-desoxy-4-O-(β-D-galactopyranosyl)-α-D-glucopyranosid

Guidance literature:: With sodium methylate; In methanol; for 12h; Yield given;

Reference yield:

: 55287-49-5
benzyl 2-acetamido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranoside

: 70209-54-0
Benzyl-2-acetamido-3,6-di-O-benzyl-2-desoxy-4-O-(β-D-galactopyranosyl)-α-D-glucopyranosid

Guidance literature:: Multi-step reaction with 2 steps

1: 62 percent / mercury(II) cyanide / benzene / 30 h / Heating

2: 1M sodium methoxide / methanol / 0.5 h / Ambient temperature

With sodium methylate; mercury(II) cyanide; In methanol; benzene;
DOI:10.1039/P19810001626

Reference yield:

: 14146-27-1
benzyl 3-O-benzyl-2-acetamido-2-deoxy-α-D-glucopyranoside

: 70209-54-0
Benzyl-2-acetamido-3,6-di-O-benzyl-2-desoxy-4-O-(β-D-galactopyranosyl)-α-D-glucopyranosid

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) bis(tributylstannyl) oxidel, 2.) tetrabutylammonium bromide / 1.) toluene, reflux, 4 h, 2.) 80 deg C, 48 h

2: 62 percent / mercury(II) cyanide / benzene / 30 h / Heating

3: 1M sodium methoxide / methanol / 0.5 h / Ambient temperature

With tetrabutylammomium bromide; sodium methylate; mercury(II) cyanide; bis(tri-n-butyltin)oxide; In methanol; benzene;
DOI:10.1039/P19810001626