Technology Process of N-(1-Amino-6-phenoxy-5-indanyl)-methansulfonamid, Acetat
There total 8 articles about N-(1-Amino-6-phenoxy-5-indanyl)-methansulfonamid, Acetat which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
ammonia; hydrogen;
nickel;
In
methanol;
at 90 ℃;
under 55163.1 - 73550.8 Torr;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 75 percent / 2 h / 155 - 160 °C
2: 59 percent / O3 / CHCl3 / 0.5 h / -40 °C
3: 89 percent / N2H4*H2O / Raney-nickel / dioxane; ethanol / 1.) 50 deg C, 1 h; 2.) reflux, 30 min
4: 82 percent / pyridine / 1.) 0 deg C, 1 h; 2.) 20 deg C, 2 h
5: 99 percent / NH2-OH*HCl, NaOAc / methanol; H2O / 3 h / Heating
6: 19 percent / NH3, H2 / Raney-nickel / methanol / 90 °C / 55163.1 - 73550.8 Torr
With
hydroxylamine hydrochloride; ammonia; hydrogen; sodium acetate; ozone; hydrazine hydrate;
nickel;
In
1,4-dioxane; pyridine; methanol; ethanol; chloroform; water;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 59 percent / O3 / CHCl3 / 0.5 h / -40 °C
2: 89 percent / N2H4*H2O / Raney-nickel / dioxane; ethanol / 1.) 50 deg C, 1 h; 2.) reflux, 30 min
3: 82 percent / pyridine / 1.) 0 deg C, 1 h; 2.) 20 deg C, 2 h
4: 99 percent / NH2-OH*HCl, NaOAc / methanol; H2O / 3 h / Heating
5: 19 percent / NH3, H2 / Raney-nickel / methanol / 90 °C / 55163.1 - 73550.8 Torr
With
hydroxylamine hydrochloride; ammonia; hydrogen; sodium acetate; ozone; hydrazine hydrate;
nickel;
In
1,4-dioxane; pyridine; methanol; ethanol; chloroform; water;
