alpha-(3-thienyl)-alpha,alpha-cyclotetramethylene-acetonitrile

Base Information

Chemical Name:alpha-(3-thienyl)-alpha,alpha-cyclotetramethylene-acetonitrile
CAS No.:55504-26-2
Molecular Formula:C₁₀H₁₁NS
Molecular Weight:177.27
Hs Code.:
Mol file:55504-26-2.mol

Synonyms:alpha-(3-thienyl)-alpha,alpha-cyclotetramethylene-acetonitrile

Suppliers and Price of alpha-(3-thienyl)-alpha,alpha-cyclotetramethylene-acetonitrile

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 3 raw suppliers

Chemical Property of alpha-(3-thienyl)-alpha,alpha-cyclotetramethylene-acetonitrile

Chemical Property:

Boiling Point:105-107 °C(Press: 0.2 Torr)
Density:1.14±0.1 g/cm3(Predicted)

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of alpha-(3-thienyl)-alpha,alpha-cyclotetramethylene-acetonitrile

There total 1 articles about alpha-(3-thienyl)-alpha,alpha-cyclotetramethylene-acetonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 110-52-1
1,4-dibromo-butane

: 13781-53-8
(thiophen-3-yl)acetonitrile

: 55504-26-2
alpha-(3-thienyl)-alpha,alpha-cyclotetramethylene-acetonitrile

Guidance literature:: With hydrogenchloride; In N-methyl-acetamide;

Reference yield:

: 55504-26-2
alpha-(3-thienyl)-alpha,alpha-cyclotetramethylene-acetonitrile

: 1-(2,6-Diisopropyl-phenyl)-3-(1-thiophen-2-yl-cyclopentylmethyl)-urea

Guidance literature:: Multi-step reaction with 2 steps

1: H₂, NH₃ / Raney Ni / methanol / 40 h / 20 - 40 °C / 2585.7 Torr

2: ethyl acetate / 20 h / Ambient temperature

With ammonia; hydrogen; nickel; In methanol; ethyl acetate;
DOI:10.1021/jm00074a011

Reference yield:

: 55504-26-2
alpha-(3-thienyl)-alpha,alpha-cyclotetramethylene-acetonitrile

: 73812-19-8
1-Thiophen-3-yl-cyclopentanecarbonyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1: 62 percent / potassium hydroxide / bis-(2-hydroxy-ethyl) ether / 6 h / 130 °C

2: thionyl chloride / benzene / Heating

With potassium hydroxide; thionyl chloride; In diethylene glycol; benzene;