tert-butyl (1R,2S)-1-allyl-2-((S)-1-(tert-butyldiphenylsilyloxy)propan-2-yl)cyclopentylcarbamate

Base Information

Chemical Name:tert-butyl (1R,2S)-1-allyl-2-((S)-1-(tert-butyldiphenylsilyloxy)propan-2-yl)cyclopentylcarbamate
CAS No.:1148178-19-1
Molecular Formula:C₃₂H₄₇NO₃Si
Molecular Weight:521.816
Hs Code.:

Synonyms:tert-butyl (1R,2S)-1-allyl-2-((S)-1-(tert-butyldiphenylsilyloxy)propan-2-yl)cyclopentylcarbamate

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Chemical Property of tert-butyl (1R,2S)-1-allyl-2-((S)-1-(tert-butyldiphenylsilyloxy)propan-2-yl)cyclopentylcarbamate

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Technology Process of tert-butyl (1R,2S)-1-allyl-2-((S)-1-(tert-butyldiphenylsilyloxy)propan-2-yl)cyclopentylcarbamate

There total 1 articles about tert-butyl (1R,2S)-1-allyl-2-((S)-1-(tert-butyldiphenylsilyloxy)propan-2-yl)cyclopentylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1148178-18-0
tert-butyl (1R,2S)-1-allyl-2-((S)-1-hydroxypropan-2-yl)cyclopentylcarbamate

: 58479-61-1
tert-butylchlorodiphenylsilane

: 1148178-19-1
tert-butyl (1R,2S)-1-allyl-2-((S)-1-(tert-butyldiphenylsilyloxy)propan-2-yl)cyclopentylcarbamate

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide; at 0 - 20 ℃;
DOI:10.1021/ol900447n

Reference yield: 76.0%

: 1148178-19-1
tert-butyl (1R,2S)-1-allyl-2-((S)-1-(tert-butyldiphenylsilyloxy)propan-2-yl)cyclopentylcarbamate

: 6213-88-3,6214-23-9,89033-13-6
3-iodoacrylic acid methyl ester

: 1148178-20-4
methyl (E)-6-((1R,2S)-1-(tert-butoxycarbonylamino)-2-((S)-1-(tert-butyldiphenylsilyloxy)propan-2-yl)cyclopentyl)hex-2-enoate

Guidance literature:: tert-butyl (1R,2S)-1-allyl-2-((S)-1-(tert-butyldiphenylsilyloxy)propan-2-yl)cyclopentylcarbamate; With 9-bora-bicyclo[3.3.1]nonane; In tetrahydrofuran; at 20 ℃; for 1.5h;

3-iodoacrylic acid methyl ester; With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; triphenyl-arsane; caesium carbonate; In tetrahydrofuran; water; N,N-dimethyl-formamide; at 20 ℃; for 2h;
DOI:10.1021/ol900447n

Reference yield:

: diethyl 2-(3-iodoallylidene)malonate

: 1148178-19-1
tert-butyl (1R,2S)-1-allyl-2-((S)-1-(tert-butyldiphenylsilyloxy)propan-2-yl)cyclopentylcarbamate

: C₄₂H₆₁NO₇Si

Guidance literature:: tert-butyl (1R,2S)-1-allyl-2-((S)-1-(tert-butyldiphenylsilyloxy)propan-2-yl)cyclopentylcarbamate; With 9-bora-bicyclo[3.3.1]nonane; In tetrahydrofuran; at 20 ℃; for 1.5h;

diethyl 2-(3-iodoallylidene)malonate; With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; triphenyl-arsane; caesium carbonate; In tetrahydrofuran; water; N,N-dimethyl-formamide; at 20 ℃; for 3h;
DOI:10.1021/ol900447n