(+/-)-(E)-4-(4-(hydroxymethyl)-1H-1,2,3-triazol-1-yl)butyl 5-hydroxy-4-(4-methoxybenzyloxy)-4-methylpent-2-enoate

Base Information

Chemical Name:(+/-)-(E)-4-(4-(hydroxymethyl)-1H-1,2,3-triazol-1-yl)butyl 5-hydroxy-4-(4-methoxybenzyloxy)-4-methylpent-2-enoate
CAS No.:1263068-06-9
Molecular Formula:C₂₁H₂₉N₃O₆
Molecular Weight:419.478
Hs Code.:

Synonyms:(+/-)-(E)-4-(4-(hydroxymethyl)-1H-1,2,3-triazol-1-yl)butyl 5-hydroxy-4-(4-methoxybenzyloxy)-4-methylpent-2-enoate

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Chemical Property of (+/-)-(E)-4-(4-(hydroxymethyl)-1H-1,2,3-triazol-1-yl)butyl 5-hydroxy-4-(4-methoxybenzyloxy)-4-methylpent-2-enoate

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Technology Process of (+/-)-(E)-4-(4-(hydroxymethyl)-1H-1,2,3-triazol-1-yl)butyl 5-hydroxy-4-(4-methoxybenzyloxy)-4-methylpent-2-enoate

There total 1 articles about (+/-)-(E)-4-(4-(hydroxymethyl)-1H-1,2,3-triazol-1-yl)butyl 5-hydroxy-4-(4-methoxybenzyloxy)-4-methylpent-2-enoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 1263068-05-8
(+/-)-(E)-4-(4-((tert-butyldimethylsilyloxy)methyl)-1H-1,2,3-triazol-1-yl)butyl 5-(tert-butyldimethylsilyloxy)-4-(4-methoxybenzyloxy)-4-methylpent-2-enoate

: 1263068-06-9
(+/-)-(E)-4-(4-(hydroxymethyl)-1H-1,2,3-triazol-1-yl)butyl 5-hydroxy-4-(4-methoxybenzyloxy)-4-methylpent-2-enoate

Guidance literature:: (+/-)-(E)-4-(4-((tert-butyldimethylsilyloxy)methyl)-1H-1,2,3-triazol-1-yl)butyl 5-(tert-butyldimethylsilyloxy)-4-(4-methoxybenzyloxy)-4-methylpent-2-enoate; With tetrabutyl ammonium fluoride; In tetrahydrofuran; for 4.5h;

With ammonium chloride; In tetrahydrofuran; water; ethyl acetate;
DOI:10.1016/j.tet.2010.10.071

Reference yield: 100.0%

: 1263068-06-9
(+/-)-(E)-4-(4-(hydroxymethyl)-1H-1,2,3-triazol-1-yl)butyl 5-hydroxy-4-(4-methoxybenzyloxy)-4-methylpent-2-enoate

: 1263068-17-2
(+/-)-(E)-4-(4-formyl-1H-1,2,3-triazol-1-yl)butyl 4-(4-methoxybenzyloxy)-4-methyl-5-oxopent-2-enoate

Guidance literature:: With 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In acetonitrile; at 55 ℃; for 3.5h;
DOI:10.1016/j.tet.2010.10.071

Reference yield: 51.0%

: 1263068-06-9
(+/-)-(E)-4-(4-(hydroxymethyl)-1H-1,2,3-triazol-1-yl)butyl 5-hydroxy-4-(4-methoxybenzyloxy)-4-methylpent-2-enoate

: C₂₁H₂₇N₃O₇S

Guidance literature:: With dmap; thionyl chloride; triethylamine; In dichloromethane; at 20 ℃; for 1.16667h; Inert atmosphere;
DOI:10.1016/j.tet.2010.10.071