(4S,5R)-N-(2-phenylbenzoyl)-2,2,5-trimethyl-4-oxazolidinecarboxylic acid

Base Information

Chemical Name:(4S,5R)-N-(2-phenylbenzoyl)-2,2,5-trimethyl-4-oxazolidinecarboxylic acid
CAS No.:438620-48-5
Molecular Formula:C₂₀H₂₁NO₄
Molecular Weight:339.391
Hs Code.:

Synonyms:(4S,5R)-N-(2-phenylbenzoyl)-2,2,5-trimethyl-4-oxazolidinecarboxylic acid

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Chemical Property of (4S,5R)-N-(2-phenylbenzoyl)-2,2,5-trimethyl-4-oxazolidinecarboxylic acid

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Technology Process of (4S,5R)-N-(2-phenylbenzoyl)-2,2,5-trimethyl-4-oxazolidinecarboxylic acid

There total 4 articles about (4S,5R)-N-(2-phenylbenzoyl)-2,2,5-trimethyl-4-oxazolidinecarboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 438620-47-4
3-(o-phenylbenzoyl)-2,2,5R-trimethyloxazolidine-4S-carboxylic acid methyl ester

: 438620-48-5
(4S,5R)-N-(2-phenylbenzoyl)-2,2,5-trimethyl-4-oxazolidinecarboxylic acid

Guidance literature:: With sodium hydroxide; In tetrahydrofuran; water; at 20 ℃; for 3h;
DOI:10.1021/ol025865r

Reference yield:

: 438620-45-2
2S-(o-phenylbenzoyl)amino-3R-hydroxybutylic acid methyl ester

: 438620-48-5
(4S,5R)-N-(2-phenylbenzoyl)-2,2,5-trimethyl-4-oxazolidinecarboxylic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 69 percent / p-TsOH / benzene; CHCl₃

2: 99 percent / NaOH / tetrahydrofuran; H₂O / 3 h / 20 °C

With sodium hydroxide; toluene-4-sulfonic acid; In tetrahydrofuran; chloroform; water; benzene;
DOI:10.1021/ol025865r

Reference yield:

: 14002-52-9
o-phenylbenzoyl chloride

: 438620-48-5
(4S,5R)-N-(2-phenylbenzoyl)-2,2,5-trimethyl-4-oxazolidinecarboxylic acid

Guidance literature:: Multi-step reaction with 4 steps

1: 95 percent / NaOH

2: 92.8 percent / K₂CO₃ / dimethylformamide

3: 69 percent / p-TsOH / benzene; CHCl₃

4: 99 percent / NaOH / tetrahydrofuran; H₂O / 3 h / 20 °C

With sodium hydroxide; potassium carbonate; toluene-4-sulfonic acid; In tetrahydrofuran; chloroform; water; N,N-dimethyl-formamide; benzene;
DOI:10.1021/ol025865r