5-tert-butyl-N,N'-bis-[3-{2-[2-(4-toluenesulfonyloxy)ethoxy]ethoxy}phenyl]-1,3-benzenediamide

Base Information

Chemical Name:5-tert-butyl-N,N'-bis-[3-{2-[2-(4-toluenesulfonyloxy)ethoxy]ethoxy}phenyl]-1,3-benzenediamide
CAS No.:835875-12-2
Molecular Formula:C₄₆H₅₂N₂O₁₂S₂
Molecular Weight:889.057
Hs Code.:

Synonyms:5-tert-butyl-N,N'-bis-[3-{2-[2-(4-toluenesulfonyloxy)ethoxy]ethoxy}phenyl]-1,3-benzenediamide

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Chemical Property of 5-tert-butyl-N,N'-bis-[3-{2-[2-(4-toluenesulfonyloxy)ethoxy]ethoxy}phenyl]-1,3-benzenediamide

Chemical Property:

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Technology Process of 5-tert-butyl-N,N'-bis-[3-{2-[2-(4-toluenesulfonyloxy)ethoxy]ethoxy}phenyl]-1,3-benzenediamide

There total 4 articles about 5-tert-butyl-N,N'-bis-[3-{2-[2-(4-toluenesulfonyloxy)ethoxy]ethoxy}phenyl]-1,3-benzenediamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 835875-09-7
5-tert-butyl-N,N'-bis-{3-[2-(2-hydroxyethoxy)ethoxy]phenyl}-1,3-benzenediamide

: 98-59-9
p-toluenesulfonyl chloride

: 835875-12-2
5-tert-butyl-N,N'-bis-[3-{2-[2-(4-toluenesulfonyloxy)ethoxy]ethoxy}phenyl]-1,3-benzenediamide

Guidance literature:: With triethylamine; In dichloromethane; for 40h;
DOI:10.1039/b411583j

Reference yield:

: 835875-06-4
5-tert-butyl-N,N'-bis(3-hydroxyphenyl)-1,3-benzenediamide

: 835875-12-2
5-tert-butyl-N,N'-bis-[3-{2-[2-(4-toluenesulfonyloxy)ethoxy]ethoxy}phenyl]-1,3-benzenediamide

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / K₂CO₃ / acetonitrile / 120 h / Heating

2: 63 percent / Et₃N / CH₂Cl₂ / 40 h

With potassium carbonate; triethylamine; In dichloromethane; acetonitrile;
DOI:10.1039/b411583j

Reference yield:

: 591-27-5
m-Hydroxyaniline

: 835875-12-2
5-tert-butyl-N,N'-bis-[3-{2-[2-(4-toluenesulfonyloxy)ethoxy]ethoxy}phenyl]-1,3-benzenediamide

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / Et₃N / acetonitrile

2: 95 percent / K₂CO₃ / acetonitrile / 120 h / Heating

3: 63 percent / Et₃N / CH₂Cl₂ / 40 h

With potassium carbonate; triethylamine; In dichloromethane; acetonitrile;
DOI:10.1039/b411583j