Technology Process of C11H12N4O2S
There total 4 articles about C11H12N4O2S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: platinum(IV) oxide; hydrogen / ethanol / 1 h / 760.05 Torr
2: palladium diacetate; caesium carbonate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene / 1,4-dioxane / 4 h / 85 °C / Inert atmosphere
3: methoxybenzene; trifluoroacetic acid / dichloromethane / 24 h / 25 - 40 °C
With
platinum(IV) oxide; hydrogen; palladium diacetate; caesium carbonate; methoxybenzene; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; trifluoroacetic acid;
In
1,4-dioxane; ethanol; dichloromethane;
2: Buchwald-Hartwig coupling;
DOI:10.1016/j.tetlet.2011.02.034
- Guidance literature:
-
Multi-step reaction with 4 steps
1: potassium carbonate; sodium iodide / butanone / 16 h / 80 °C
2: platinum(IV) oxide; hydrogen / ethanol / 1 h / 760.05 Torr
3: palladium diacetate; caesium carbonate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene / 1,4-dioxane / 4 h / 85 °C / Inert atmosphere
4: methoxybenzene; trifluoroacetic acid / dichloromethane / 24 h / 25 - 40 °C
With
platinum(IV) oxide; hydrogen; palladium diacetate; potassium carbonate; caesium carbonate; methoxybenzene; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; trifluoroacetic acid; sodium iodide;
In
1,4-dioxane; ethanol; dichloromethane; butanone;
3: Buchwald-Hartwig coupling;
DOI:10.1016/j.tetlet.2011.02.034