(1S,3R)-3-phthalimidocyclohexanecarboxylic acid

Base Information

Chemical Name:(1S,3R)-3-phthalimidocyclohexanecarboxylic acid
CAS No.:81131-38-6
Molecular Formula:C₁₅H₁₅NO₄
Molecular Weight:273.288
Hs Code.:

Synonyms:(1S,3R)-3-phthalimidocyclohexanecarboxylic acid

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Chemical Property of (1S,3R)-3-phthalimidocyclohexanecarboxylic acid

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Technology Process of (1S,3R)-3-phthalimidocyclohexanecarboxylic acid

There total 3 articles about (1S,3R)-3-phthalimidocyclohexanecarboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 81202-30-4
(1S,5S)-5-(1,3-Dioxo-1,3-dihydro-isoindol-2-yl)-cyclohex-3-enecarboxylic acid

: 81131-38-6
(1S,3R)-3-phthalimidocyclohexanecarboxylic acid

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; for 2h; under 760 Torr;
DOI:10.1071/CH9812231

Reference yield:

: 81086-72-8
5-Bromo-cyclohex-3-enecarboxylic acid ethyl ester

: 81131-38-6
(1S,3R)-3-phthalimidocyclohexanecarboxylic acid

Guidance literature:: Multi-step reaction with 4 steps

1: 57 percent / N-methylpyrrolidone / 2.5 h / 80 °C

2: 72 percent / conc. HCl / dioxane; H₂O / 6 h / Heating

4: 200 mg / H₂ / 10percent Pd/C / methanol / 2 h / 760 Torr

With 1-methyl-pyrrolidin-2-one; hydrogenchloride; hydrogen; palladium on activated charcoal; In 1,4-dioxane; methanol; water;
DOI:10.1071/CH9812231

Reference yield:

: 81201-62-9,81202-29-1,81202-30-4
(d,l)-cis-3-phthalimidocyclohex-4-ene-1-carboxylic acid

: 81131-38-6
(1S,3R)-3-phthalimidocyclohexanecarboxylic acid

Guidance literature:: Multi-step reaction with 2 steps

2: 200 mg / H₂ / 10percent Pd/C / methanol / 2 h / 760 Torr

With hydrogen; palladium on activated charcoal; In methanol;
DOI:10.1071/CH9812231