N-carbamimidoyl-4-(2,3,4-trimethoxybenzoyl)piperazine-1-carboximidamide hydrochloride

Base Information

Chemical Name:N-carbamimidoyl-4-(2,3,4-trimethoxybenzoyl)piperazine-1-carboximidamide hydrochloride
CAS No.:1383744-10-2
Molecular Formula:C₁₆H₂₄N₆O₄*ClH
Molecular Weight:400.865
Hs Code.:

Synonyms:N-carbamimidoyl-4-(2,3,4-trimethoxybenzoyl)piperazine-1-carboximidamide hydrochloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-carbamimidoyl-4-(2,3,4-trimethoxybenzoyl)piperazine-1-carboximidamide hydrochloride

Chemical Property:

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Technology Process of N-carbamimidoyl-4-(2,3,4-trimethoxybenzoyl)piperazine-1-carboximidamide hydrochloride

There total 3 articles about N-carbamimidoyl-4-(2,3,4-trimethoxybenzoyl)piperazine-1-carboximidamide hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 1-(2,3,4-trimethoxybenzoyl)piperazine hydrochloride

: 127099-85-8,780722-26-1,461-58-5
N-Cyanoguanidine

: 1383744-10-2
N-carbamimidoyl-4-(2,3,4-trimethoxybenzoyl)piperazine-1-carboximidamide hydrochloride

Guidance literature:: In butan-1-ol; for 10h; Reflux;

Reference yield:

: 573-11-5
2,3,4-Trimethoxy-benzoic acid

: 1383744-10-2
N-carbamimidoyl-4-(2,3,4-trimethoxybenzoyl)piperazine-1-carboximidamide hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydroxide; thionyl chloride / water; benzene / 2 h / Reflux

2: acetic acid / water; tetrahydrofuran / 10 - 15 °C

3: butan-1-ol / 10 h / Reflux

With thionyl chloride; acetic acid; sodium hydroxide; In tetrahydrofuran; water; butan-1-ol; benzene;

Reference yield:

: 7169-07-5
3,4,5-(trimethoxy)benzoyl chloride

: 1383744-10-2
N-carbamimidoyl-4-(2,3,4-trimethoxybenzoyl)piperazine-1-carboximidamide hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: acetic acid / water; tetrahydrofuran / 10 - 15 °C

2: butan-1-ol / 10 h / Reflux

With acetic acid; In tetrahydrofuran; water; butan-1-ol;