diisopropyl (R)-[(2-triphenylmethoxy-1-methylethyloxy)-methyl]phosphonate

Base Information

Chemical Name:diisopropyl (R)-[(2-triphenylmethoxy-1-methylethyloxy)-methyl]phosphonate
CAS No.:1259531-39-9
Molecular Formula:C₂₉H₃₇O₅P
Molecular Weight:496.584
Hs Code.:

Synonyms:diisopropyl (R)-[(2-triphenylmethoxy-1-methylethyloxy)-methyl]phosphonate

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Chemical Property of diisopropyl (R)-[(2-triphenylmethoxy-1-methylethyloxy)-methyl]phosphonate

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Technology Process of diisopropyl (R)-[(2-triphenylmethoxy-1-methylethyloxy)-methyl]phosphonate

There total 2 articles about diisopropyl (R)-[(2-triphenylmethoxy-1-methylethyloxy)-methyl]phosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 35717-98-7
bis(2-propyl)-p-toluenesulfonyloxymethylphosphonate

: 20263-26-7
(R)-1-triphenylmethylmethoxy-2-propanol

: 1259531-39-9
diisopropyl (R)-[(2-triphenylmethoxy-1-methylethyloxy)-methyl]phosphonate

Guidance literature:: (R)-1-triphenylmethylmethoxy-2-propanol; With sodium hydride; In tetrahydrofuran; mineral oil; at 20 ℃; for 6.16667h; Cooling with ice; Reflux;

bis(2-propyl)-p-toluenesulfonyloxymethylphosphonate; In tetrahydrofuran; mineral oil; at 5 - 20 ℃; for 2h;

Reference yield:

: 76-83-5
trityl chloride

: 1259531-39-9
diisopropyl (R)-[(2-triphenylmethoxy-1-methylethyloxy)-methyl]phosphonate

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine; 2-(Dimethylamino)pyridine / dichloromethane / 20 °C / Cooling with ice

2.1: sodium hydride / tetrahydrofuran; mineral oil / 6.17 h / 20 °C / Cooling with ice; Reflux

2.2: 2 h / 5 - 20 °C

With 2-(Dimethylamino)pyridine; sodium hydride; triethylamine; In tetrahydrofuran; dichloromethane; mineral oil;