2,6-bis(3-hydroxy-3-oxo-1-phenylprop-1-yl)pyrrolo[3,4-f]isoindole-1,3,5,7(2H,6H)-tetraone

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Chemical Name:2,6-bis(3-hydroxy-3-oxo-1-phenylprop-1-yl)pyrrolo[3,4-f]isoindole-1,3,5,7(2H,6H)-tetraone
CAS No.:1133768-70-3
Molecular Formula:C₂₈H₂₀N₂O₈
Molecular Weight:512.475
Hs Code.:

Synonyms:2,6-bis(3-hydroxy-3-oxo-1-phenylprop-1-yl)pyrrolo[3,4-f]isoindole-1,3,5,7(2H,6H)-tetraone

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Chemical Property of 2,6-bis(3-hydroxy-3-oxo-1-phenylprop-1-yl)pyrrolo[3,4-f]isoindole-1,3,5,7(2H,6H)-tetraone

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Technology Process of 2,6-bis(3-hydroxy-3-oxo-1-phenylprop-1-yl)pyrrolo[3,4-f]isoindole-1,3,5,7(2H,6H)-tetraone

There total 1 articles about 2,6-bis(3-hydroxy-3-oxo-1-phenylprop-1-yl)pyrrolo[3,4-f]isoindole-1,3,5,7(2H,6H)-tetraone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 89-32-7,34527-94-1
Pyromellitic dianhydride

: 3646-50-2
3-Amino-3-phenylpropionic acid

: 1133768-70-3
2,6-bis(3-hydroxy-3-oxo-1-phenylprop-1-yl)pyrrolo[3,4-f]isoindole-1,3,5,7(2H,6H)-tetraone

Guidance literature:: In nitrobenzene; at 155 - 165 ℃; for 1h;
DOI:10.1007/s11172-007-0394-4

Reference yield: 76.0%

: 186581-53-3,908094-01-9,334-88-3
diazomethane

: 1133768-70-3
2,6-bis(3-hydroxy-3-oxo-1-phenylprop-1-yl)pyrrolo[3,4-f]isoindole-1,3,5,7(2H,6H)-tetraone

: 1133768-73-6
2,6-bis(4-diazo-3-oxo-1-phenylbut-1-yl)pyrrolo[3,4-f]isoindole-1,3,5,7(2H,6H)-tetraone

Guidance literature:: 2,6-bis(3-hydroxy-3-oxo-1-phenylprop-1-yl)pyrrolo[3,4-f]isoindole-1,3,5,7(2H,6H)-tetraone; With 4-methyl-morpholine; methyl chloroformate; In tetrahydrofuran; for 0.5h;

diazomethane; In tetrahydrofuran; at 0 ℃; Further stages.;
DOI:10.1007/s11172-007-0394-4