2-azido-4-methoxyphenylboronic acid pinacolate ester

Base Information

Chemical Name:2-azido-4-methoxyphenylboronic acid pinacolate ester
CAS No.:1579291-79-4
Molecular Formula:C₁₃H₁₈BN₃O₃
Molecular Weight:275.115
Hs Code.:

Synonyms:2-azido-4-methoxyphenylboronic acid pinacolate ester

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Chemical Property of 2-azido-4-methoxyphenylboronic acid pinacolate ester

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Technology Process of 2-azido-4-methoxyphenylboronic acid pinacolate ester

There total 4 articles about 2-azido-4-methoxyphenylboronic acid pinacolate ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 1310404-85-3
2-amino-4-methoxyphenylboronic acid pinacolate ester

: 1579291-79-4
2-azido-4-methoxyphenylboronic acid pinacolate ester

Guidance literature:: With 2-Methyl-2-nitropropane; trimethylsilylazide; In acetonitrile; at 0 - 20 ℃; for 1.5h; Inert atmosphere;
DOI:10.1021/ol5010615

Reference yield:

: 59557-92-5
2-bromo-5-methoxyaniline

: 1579291-79-4
2-azido-4-methoxyphenylboronic acid pinacolate ester

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 1,4-dioxane / 12 h / 120 °C / Inert atmosphere

2: 2-Methyl-2-nitropropane; trimethylsilylazide / acetonitrile / 1.5 h / 0 - 20 °C / Inert atmosphere

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; 2-Methyl-2-nitropropane; trimethylsilylazide; triethylamine; In 1,4-dioxane; acetonitrile;
DOI:10.1021/jo500252e

Reference yield:

: 25015-63-8
4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane

: 1579291-79-4
2-azido-4-methoxyphenylboronic acid pinacolate ester

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 1,4-dioxane / 12 h / 120 °C / Inert atmosphere

2: 2-Methyl-2-nitropropane; trimethylsilylazide / acetonitrile / 1.5 h / 0 - 20 °C / Inert atmosphere

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; 2-Methyl-2-nitropropane; trimethylsilylazide; triethylamine; In 1,4-dioxane; acetonitrile;
DOI:10.1021/jo500252e