m,m'-di(dodecyloxy)acetophenone

Base Information

• Chemical Name: m,m'-di(dodecyloxy)acetophenone
• CAS No.: 208930-08-9
• Molecular Formula: C₃₂H₅₆O₃
• Molecular Weight: 488.795
• Mol file: 208930-08-9.mol

Synonyms:m,m'-di(dodecyloxy)acetophenone

Chemical Property of m,m'-di(dodecyloxy)acetophenone

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of m,m'-di(dodecyloxy)acetophenone

There total 1 articles about m,m'-di(dodecyloxy)acetophenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

3,5-dihydroxyacetophenone (51863-60-6) + 1-dodecylbromide (143-15-7) → m,m'-di(dodecyloxy)acetophenone (208930-08-9)

Guidance literature:

With potassium carbonate; potassium iodide; In cyclohexanone; for 12h; Heating;

DOI:10.1039/a800035b

Reference yield: 81.0%

ethyl-2-picolinate (2524-52-9,1228273-66-2) + m,m'-di(dodecyloxy)acetophenone (208930-08-9) → C38H59NO4

Guidance literature:

m,m'-di(dodecyloxy)acetophenone; With sodium hydride; In tetrahydrofuran; mineral oil; at 20 ℃; for 1h;

ethyl-2-picolinate; In tetrahydrofuran; mineral oil; for 24h; Reflux;

DOI:10.1016/j.dyepig.2017.09.039

Reference yield: 81.0%

oxalic acid diethyl ester (95-92-1) + m,m'-di(dodecyloxy)acetophenone (208930-08-9) → 1,6-bis(m,m'-di(dodecyloxy)phenyl)hexane-1,3,4,6-tetraone

Guidance literature:

With sodium hydride; In toluene; for 10h; Heating;

DOI:10.1002/anie.200600725

upstream raw materials:

3,5-dihydroxyacetophenone

1-dodecylbromide

Downstream raw materials:

C₃₈H₅₉N₃O₂

C₇₆H₁₁₆N₆O₄Pd

C₃₈H₅₉NO₄

Refernces

• 1、 Cuerva, Cristian,Campo, Jose A.,Ovejero, Paloma,Torres, Maria R.,Cano, Mercedes. "Polycatenar pyrazole and pyrazolate ligands as building blocks of new columnar Pd(ii) metallomesogens". . p. 8849 - 8860. Retrieved 2014/06/09.