1-(1-p-chlorophenyl-5-methyl-1,2,3-triazol-4-carbonyl)-4-phenylthiosemicarbazide

Base Information

Chemical Name:1-(1-p-chlorophenyl-5-methyl-1,2,3-triazol-4-carbonyl)-4-phenylthiosemicarbazide
CAS No.:249932-40-9
Molecular Formula:C₁₇H₁₅ClN₆OS
Molecular Weight:386.865
Hs Code.:

Synonyms:1-(1-p-chlorophenyl-5-methyl-1,2,3-triazol-4-carbonyl)-4-phenylthiosemicarbazide

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Chemical Property of 1-(1-p-chlorophenyl-5-methyl-1,2,3-triazol-4-carbonyl)-4-phenylthiosemicarbazide

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Technology Process of 1-(1-p-chlorophenyl-5-methyl-1,2,3-triazol-4-carbonyl)-4-phenylthiosemicarbazide

There total 3 articles about 1-(1-p-chlorophenyl-5-methyl-1,2,3-triazol-4-carbonyl)-4-phenylthiosemicarbazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 103-72-0
phenyl isothiocyanate

: 242145-47-7
5-methyl-1-(4-chlorophenyl)-1H-1,2,3-triazole-4-carbohydrazide

: 249932-40-9
1-(1-p-chlorophenyl-5-methyl-1,2,3-triazol-4-carbonyl)-4-phenylthiosemicarbazide

Guidance literature:: In ethanol; for 4h; Heating;

Reference yield:

: 20725-33-1
1-(4-chlorophenyl)-5-methyl-1H-1,2,3-triazole-4-carboxylic acid

: 249932-40-9
1-(1-p-chlorophenyl-5-methyl-1,2,3-triazol-4-carbonyl)-4-phenylthiosemicarbazide

Guidance literature:: Multi-step reaction with 3 steps

1: H₂SO₄

2: 86 percent / hydrazine hydrate / ethanol / 12 h / Heating

3: 70 percent / ethanol / 4 h / Heating

With sulfuric acid; hydrazine hydrate; In ethanol; 1: Esterification / 2: Substitution / 3: Addition;

Reference yield:

: 91396-26-8
ethyl 1-(4-chlorophenyl)-5-methyl-1H-1,2,3-triazole-4-carboxylate

: 249932-40-9
1-(1-p-chlorophenyl-5-methyl-1,2,3-triazol-4-carbonyl)-4-phenylthiosemicarbazide

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / hydrazine hydrate / ethanol / 12 h / Heating

2: 70 percent / ethanol / 4 h / Heating

With hydrazine hydrate; In ethanol; 1: Substitution / 2: Addition;