(2S)-1-(hexyloxy)-3-<(4-methoxyphenyl)diphenylmethoxy>-2-propyl p-toluenesulfonate

Base Information

Chemical Name:(2S)-1-(hexyloxy)-3-<(4-methoxyphenyl)diphenylmethoxy>-2-propyl p-toluenesulfonate
CAS No.:161392-02-5
Molecular Formula:C₃₆H₄₂O₆S
Molecular Weight:602.792
Hs Code.:

Synonyms:(2S)-1-(hexyloxy)-3-<(4-methoxyphenyl)diphenylmethoxy>-2-propyl p-toluenesulfonate

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Chemical Property of (2S)-1-(hexyloxy)-3-<(4-methoxyphenyl)diphenylmethoxy>-2-propyl p-toluenesulfonate

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Technology Process of (2S)-1-(hexyloxy)-3-<(4-methoxyphenyl)diphenylmethoxy>-2-propyl p-toluenesulfonate

There total 4 articles about (2S)-1-(hexyloxy)-3-<(4-methoxyphenyl)diphenylmethoxy>-2-propyl p-toluenesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 98-59-9
p-toluenesulfonyl chloride

: 161392-01-4
(2S)-1-(hexyloxy)-3-<(4-methoxyphenyl)diphenylmethoxy>-2-propanol

: 161392-02-5
(2S)-1-(hexyloxy)-3-<(4-methoxyphenyl)diphenylmethoxy>-2-propyl p-toluenesulfonate

Guidance literature:: With pyridine; In dichloromethane; at 25 ℃; for 14h;
DOI:10.1021/jm00050a009

Reference yield:

: 111-25-1
1-bromo-hexane

: 161392-02-5
(2S)-1-(hexyloxy)-3-<(4-methoxyphenyl)diphenylmethoxy>-2-propyl p-toluenesulfonate

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) NaH / 1.) DMF, 45 min, 2.) DMF, 25 deg C, 14 h

2: 100 percent / 1 N HCl / methanol / 24 h / 25 °C

3: 92 percent / pyridine / tetrahydrofuran / 14 h / 25 °C

4: 71 percent / pyridine / CH₂Cl₂ / 14 h / 25 °C

With pyridine; hydrogenchloride; sodium hydride; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1021/jm00050a009

Reference yield:

: 86158-13-6
(2S)-3-(hexyloxy)-1,2-propanediol

: 161392-02-5
(2S)-1-(hexyloxy)-3-<(4-methoxyphenyl)diphenylmethoxy>-2-propyl p-toluenesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / pyridine / tetrahydrofuran / 14 h / 25 °C

2: 71 percent / pyridine / CH₂Cl₂ / 14 h / 25 °C

With pyridine; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jm00050a009