(4S)-tert-butyl 4-(3-(3-methoxypropoxy)-4-methoxybenzyl)-2-(diphenylmethyleneamino)-5-methylhexanoate

Base Information

Chemical Name:(4S)-tert-butyl 4-(3-(3-methoxypropoxy)-4-methoxybenzyl)-2-(diphenylmethyleneamino)-5-methylhexanoate
CAS No.:955020-76-5
Molecular Formula:C₃₆H₄₇NO₅
Molecular Weight:573.773
Hs Code.:

Synonyms:(4S)-tert-butyl 4-(3-(3-methoxypropoxy)-4-methoxybenzyl)-2-(diphenylmethyleneamino)-5-methylhexanoate

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Chemical Property of (4S)-tert-butyl 4-(3-(3-methoxypropoxy)-4-methoxybenzyl)-2-(diphenylmethyleneamino)-5-methylhexanoate

Chemical Property:

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Technology Process of (4S)-tert-butyl 4-(3-(3-methoxypropoxy)-4-methoxybenzyl)-2-(diphenylmethyleneamino)-5-methylhexanoate

There total 10 articles about (4S)-tert-butyl 4-(3-(3-methoxypropoxy)-4-methoxybenzyl)-2-(diphenylmethyleneamino)-5-methylhexanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 172900-75-3
4-methoxy-3-(3-methoxypropoxy)benzaldehyde

: 955020-76-5
(4S)-tert-butyl 4-(3-(3-methoxypropoxy)-4-methoxybenzyl)-2-(diphenylmethyleneamino)-5-methylhexanoate

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium tetrahydroborate; ethanol / 20 °C

2.1: pyridine; phosphorus tribromide / diethyl ether / 3 h / 20 °C

3.1: lithium hexamethyldisilazane / tetrahydrofuran / 0.5 h / Cooling with acetone-dry ice

3.2: 20 °C / Cooling with acetone-dry ice

4.1: lithium borohydride; water / diethyl ether / 0.67 h / 0 °C

5.1: 1H-imidazole; iodine; triphenylphosphine / dichloromethane / 3 h

6.1: lithium hexamethyldisilazane / tetrahydrofuran / 0.25 h / Cooling with acetone-dry ice

6.2: 20 °C / Cooling with acetone-dry ice

With pyridine; 1H-imidazole; sodium tetrahydroborate; lithium borohydride; ethanol; water; iodine; phosphorus tribromide; triphenylphosphine; lithium hexamethyldisilazane; In tetrahydrofuran; diethyl ether; dichloromethane;

Reference yield:

: 900811-38-3
(R)--4-(2-(iodomethyl)--3--methylbutyl)--1--methoxy-2--(3--methoxypropoxy)benzene

: 955020-76-5
(4S)-tert-butyl 4-(3-(3-methoxypropoxy)-4-methoxybenzyl)-2-(diphenylmethyleneamino)-5-methylhexanoate

Guidance literature:: N-(diphenylmethylene)glycine tert-butyl ester; With N,N,N,N,N,N-hexamethylphosphoric triamide; lithium hexamethyldisilazane; In tetrahydrofuran; for 0.25h; Cooling with acetone-dry ice;

(R)--4-(2-(iodomethyl)--3--methylbutyl)--1--methoxy-2--(3--methoxypropoxy)benzene; In tetrahydrofuran; at 20 ℃;

Reference yield:

: 900811-38-3
(R)--4-(2-(iodomethyl)--3--methylbutyl)--1--methoxy-2--(3--methoxypropoxy)benzene

: 81477-94-3
N-(diphenylmethylene)glycine tert-butyl ester

: 955020-76-5
(4S)-tert-butyl 4-(3-(3-methoxypropoxy)-4-methoxybenzyl)-2-(diphenylmethyleneamino)-5-methylhexanoate

Guidance literature:: N-(diphenylmethylene)glycine tert-butyl ester; With lithium hexamethyldisilazane; In tetrahydrofuran; for 0.25h; Cooling with acetone-dry ice;

(R)--4-(2-(iodomethyl)--3--methylbutyl)--1--methoxy-2--(3--methoxypropoxy)benzene; In tetrahydrofuran; at 20 ℃; Cooling with acetone-dry ice;