[Au₂(triphenylphosphine)2(2-((4,5-ethylenedithio)-1,3-dithiole-2-ylidene)-1,3-dithiole-4,5-dithionato)]

Base Information

• Chemical Name: [Au₂(triphenylphosphine)2(2-((4,5-ethylenedithio)-1,3-dithiole-2-ylidene)-1,3-dithiole-4,5-dithionato)]
• CAS No.: 782500-53-2
• Molecular Formula: C₄₄H₃₄Au₂P₂S₈
• Molecular Weight: 1275.16

Synonyms:[Au₂(triphenylphosphine)2(2-((4,5-ethylenedithio)-1,3-dithiole-2-ylidene)-1,3-dithiole-4,5-dithionato)]

Chemical Property of [Au₂(triphenylphosphine)2(2-((4,5-ethylenedithio)-1,3-dithiole-2-ylidene)-1,3-dithiole-4,5-dithionato)]

Chemical Property:

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Technology Process of [Au₂(triphenylphosphine)2(2-((4,5-ethylenedithio)-1,3-dithiole-2-ylidene)-1,3-dithiole-4,5-dithionato)]

There total 1 articles about [Au₂(triphenylphosphine)2(2-((4,5-ethylenedithio)-1,3-dithiole-2-ylidene)-1,3-dithiole-4,5-dithionato)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

(triphenylphosphine)gold(I) chloride (14243-64-2) + 4,5-bis(cyanoethylthio)-1,3-dithiole-2-[(4,5-ethylenedithio)-1,3-dithiole-2-ylidene] (158871-27-3) → [Au2(triphenylphosphine)2(2-((4,5-ethylenedithio)-1,3-dithiole-2-ylidene)-1,3-dithiole-4,5-dithionato)] (782500-53-2)

Guidance literature:

With Na; In methanol; ethanol; (Ar); dissolving of C8H4S8(CH2CH2CN)2 (1 mmol) in EtOH containing sodium(5 mmol); addn. with stirring of soln. of AuCl(PPh3) (2 mmol) in CH2Cl2 ; stirring for 30 min; pptn., filtration, washing with EtOH, drying in vac., elem. anal.;

DOI:10.1016/j.ica.2004.03.048

Reference yield:

[Au2(triphenylphosphine)2(2-((4,5-ethylenedithio)-1,3-dithiole-2-ylidene)-1,3-dithiole-4,5-dithionato)] (782500-53-2) → [Au2(triphenylphosphine)2(2-((4,5-ethylenedithio)-1,3-dithiole-2-ylidene)-1,3-dithiole-4,5-dithionato)](2+)

Guidance literature:

With I₂; In dichloromethane; (Ar); treatment of (PPh3)2Au2(C8H4S8) with I2 in CH2Cl2; monitoring by UV;

DOI:10.1016/j.ica.2004.03.048

Reference yield:

[Au2(triphenylphosphine)2(2-((4,5-ethylenedithio)-1,3-dithiole-2-ylidene)-1,3-dithiole-4,5-dithionato)] (782500-53-2) + 7,7',8,8'-tetracyanoquinodimethane (1518-16-7,6144-37-2) → [Au2(PPh3)2(2-((4,5-ethylenedithio)-1,3-dithiole-2-ylidene)-1,3-dithiole-4,5-dithionato)](7,7,8,8-tetracyano-p-quinodimethane)

Guidance literature:

In dichloromethane; (Ar); treatment of (PPh3)2Au2(C8H4S8) with 7,7,8,8-tetracyano-p-quinodimethane in CH2Cl2; monitoring by UV;

DOI:10.1016/j.ica.2004.03.048

upstream raw materials:

(triphenylphosphine)gold(I) chloride

4,5-bis(cyanoethylthio)-1,3-dithiole-2-[(4,5-ethylenedithio)-1,3-dithiole-2-ylidene]

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