2-{[6-(4-Methoxyphenyl)-5-hexynyl]oxy}-5-(3-carboxybenzoyl)benzenepropanoic acid

Base Information

Chemical Name:2-{[6-(4-Methoxyphenyl)-5-hexynyl]oxy}-5-(3-carboxybenzoyl)benzenepropanoic acid
CAS No.:128578-12-1
Molecular Formula:C₃₀H₂₈O₇
Molecular Weight:500.548
Hs Code.:

Synonyms:2-{[6-(4-Methoxyphenyl)-5-hexynyl]oxy}-5-(3-carboxybenzoyl)benzenepropanoic acid

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Chemical Property of 2-{[6-(4-Methoxyphenyl)-5-hexynyl]oxy}-5-(3-carboxybenzoyl)benzenepropanoic acid

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Technology Process of 2-{[6-(4-Methoxyphenyl)-5-hexynyl]oxy}-5-(3-carboxybenzoyl)benzenepropanoic acid

There total 11 articles about 2-{[6-(4-Methoxyphenyl)-5-hexynyl]oxy}-5-(3-carboxybenzoyl)benzenepropanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 128577-87-7
2-{[6-(4-Methoxyphenyl)-5-hexynyl]oxy}-5-[3-(ethoxycarbonyl)benzoyl]benzenepropanoic acid ethyl ester

: 128578-12-1
2-{[6-(4-Methoxyphenyl)-5-hexynyl]oxy}-5-(3-carboxybenzoyl)benzenepropanoic acid

Guidance literature:: With potassium hydroxide; In ethanol; at 25 ℃; for 1h;
DOI:10.1021/jm00172a020

Reference yield: 59.0%

: 128578-12-1
2-{[6-(4-Methoxyphenyl)-5-hexynyl]oxy}-5-(3-carboxybenzoyl)benzenepropanoic acid

Guidance literature:

Reference yield:

: 104-92-7
1-bromo-4-methoxy-benzene

: 128578-12-1
2-{[6-(4-Methoxyphenyl)-5-hexynyl]oxy}-5-(3-carboxybenzoyl)benzenepropanoic acid

Guidance literature:: Multi-step reaction with 4 steps

1: 16 percent / triethylamine (TEA), tris(triphenylphosphine)palladium dichloride, copper(I) iodide / 2 h / Heating

2: triethylamine (TEA) / diethyl ether

3: 1.) 60percent sodium hydride disp. in oil / 1.) DMF, 25 deg C, 30 min, 2.) 65 deg C

4: 59 percent / KOH / aq. ethanol / 1 h / 25 °C

With potassium hydroxide; copper(l) iodide; tris(triphenylphosphine)-palladium(II) dichloride; sodium hydride; triethylamine; In diethyl ether; ethanol;
DOI:10.1021/jm00172a020