1-Benzylidene-1H-cyclobutanaphthalene

Base Information

Chemical Name:1-Benzylidene-1H-cyclobutanaphthalene
CAS No.:85924-94-3
Molecular Formula:C₁₈H₁₂
Molecular Weight:228.293
Hs Code.:

1-Benzylidene-1H-cyclobuta<de>naphthalene

Synonyms:1-Benzylidene-1H-cyclobutanaphthalene

Suppliers and Price of 1-Benzylidene-1H-cyclobutanaphthalene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-Benzylidene-1H-cyclobutanaphthalene

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Technology Process of 1-Benzylidene-1H-cyclobutanaphthalene

There total 6 articles about 1-Benzylidene-1H-cyclobutanaphthalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 54125-11-0
1-Bromo-1H-cyclobutanaphthalene

: 85924-94-3
1-Benzylidene-1H-cyclobutanaphthalene

Guidance literature:: Multi-step reaction with 2 steps

1: 97 percent / xylene / 72 h / Heating

2: 1.) tert-butyllithium / 1.) pentane, 2.) reflux

With tert.-butyl lithium; In xylene;
DOI:10.1021/ja00357a022

Reference yield:

: 24973-91-9
1H-Cyclobutanaphthalene

: 85924-94-3
1-Benzylidene-1H-cyclobutanaphthalene

Guidance literature:: Multi-step reaction with 3 steps

1: 40 percent / N-bromosuccinimide, benzoyl peroxide / CCl₄ / 4.5 h / Heating

2: 97 percent / xylene / 72 h / Heating

3: 1.) tert-butyllithium / 1.) pentane, 2.) reflux

With N-Bromosuccinimide; Perbenzoic acid; tert.-butyl lithium; In tetrachloromethane; xylene;
DOI:10.1021/ja00357a022

Reference yield:

: 85924-73-8
C₁₁H₇Li

: 85924-94-3
1-Benzylidene-1H-cyclobutanaphthalene

Guidance literature:: Multi-step reaction with 4 steps

1: 25 mg / tetrahydrofuran / 0.17 h / -78 °C

2: 40 percent / N-bromosuccinimide, benzoyl peroxide / CCl₄ / 4.5 h / Heating

3: 97 percent / xylene / 72 h / Heating

4: 1.) tert-butyllithium / 1.) pentane, 2.) reflux

With N-Bromosuccinimide; Perbenzoic acid; tert.-butyl lithium; In tetrahydrofuran; tetrachloromethane; xylene;
DOI:10.1021/ja00357a022