Technology Process of C23H23Cl2OP
There total 5 articles about C23H23Cl2OP which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
palladium diacetate; N-ethyl-N,N-diisopropylamine; 1,4-di(diphenylphosphino)-butane;
In
dimethyl sulfoxide;
at 100 ℃;
for 8h;
Inert atmosphere;
DOI:10.1021/ja312125a
- Guidance literature:
-
Multi-step reaction with 4 steps
1: [1,1'-bis(diphenylphosphino)ferrocene]nickel(II) chloride / diethyl ether / 8 h / 0 °C / Inert atmosphere; Reflux
2: boron tribromide / dichloromethane / 2 h / 0 °C / Inert atmosphere
3: N-ethyl-N,N-diisopropylamine / dichloromethane / 1 h / -78 °C
4: N-ethyl-N,N-diisopropylamine; 1,4-di(diphenylphosphino)-butane; palladium diacetate / dimethyl sulfoxide / 8 h / 100 °C / Inert atmosphere
With
[1,1'-bis(diphenylphosphino)ferrocene]nickel(II) chloride; palladium diacetate; boron tribromide; N-ethyl-N,N-diisopropylamine; 1,4-di(diphenylphosphino)-butane;
In
diethyl ether; dichloromethane; dimethyl sulfoxide;
DOI:10.1021/ja312125a
- Guidance literature:
-
Multi-step reaction with 3 steps
1: boron tribromide / dichloromethane / 2 h / 0 °C / Inert atmosphere
2: N-ethyl-N,N-diisopropylamine / dichloromethane / 1 h / -78 °C
3: N-ethyl-N,N-diisopropylamine; 1,4-di(diphenylphosphino)-butane; palladium diacetate / dimethyl sulfoxide / 8 h / 100 °C / Inert atmosphere
With
palladium diacetate; boron tribromide; N-ethyl-N,N-diisopropylamine; 1,4-di(diphenylphosphino)-butane;
In
dichloromethane; dimethyl sulfoxide;
DOI:10.1021/ja312125a
