{(1S,2R,6R)-4-Hydroxy-2,4-dimethyl-6-[1-(toluene-4-sulfonyl)-1H-indol-3-yl]-cyclohexyl}-[1-(toluene-4-sulfonyl)-1H-indol-3-yl]-methanone

Base Information

Chemical Name:{(1S,2R,6R)-4-Hydroxy-2,4-dimethyl-6-[1-(toluene-4-sulfonyl)-1H-indol-3-yl]-cyclohexyl}-[1-(toluene-4-sulfonyl)-1H-indol-3-yl]-methanone
CAS No.:114907-12-9
Molecular Formula:C₃₉H₃₈N₂O₆S₂
Molecular Weight:694.873
Hs Code.:

Synonyms:{(1S,2R,6R)-4-Hydroxy-2,4-dimethyl-6-[1-(toluene-4-sulfonyl)-1H-indol-3-yl]-cyclohexyl}-[1-(toluene-4-sulfonyl)-1H-indol-3-yl]-methanone

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Chemical Property of {(1S,2R,6R)-4-Hydroxy-2,4-dimethyl-6-[1-(toluene-4-sulfonyl)-1H-indol-3-yl]-cyclohexyl}-[1-(toluene-4-sulfonyl)-1H-indol-3-yl]-methanone

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Technology Process of {(1S,2R,6R)-4-Hydroxy-2,4-dimethyl-6-[1-(toluene-4-sulfonyl)-1H-indol-3-yl]-cyclohexyl}-[1-(toluene-4-sulfonyl)-1H-indol-3-yl]-methanone

There total 3 articles about {(1S,2R,6R)-4-Hydroxy-2,4-dimethyl-6-[1-(toluene-4-sulfonyl)-1H-indol-3-yl]-cyclohexyl}-[1-(toluene-4-sulfonyl)-1H-indol-3-yl]-methanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 114927-86-5
{(1S,2R,6R)-4,6-Dimethyl-2-[1-(toluene-4-sulfonyl)-1H-indol-3-yl]-cyclohex-3-enyl}-[1-(toluene-4-sulfonyl)-1H-indol-3-yl]-methanone

: 114907-12-9
{(1S,2R,6R)-4-Hydroxy-2,4-dimethyl-6-[1-(toluene-4-sulfonyl)-1H-indol-3-yl]-cyclohexyl}-[1-(toluene-4-sulfonyl)-1H-indol-3-yl]-methanone

Guidance literature:: With trifluoroacetic acid; for 3h; Ambient temperature;
DOI:10.1021/jo00249a009

Reference yield:

: 114907-09-4,114976-84-0
[(1R,2S,6S)-2-(1H-Indol-3-yl)-4,6-dimethyl-cyclohex-3-enyl]-[1-(toluene-4-sulfonyl)-1H-indol-3-yl]-methanone

: 114907-12-9
{(1S,2R,6R)-4-Hydroxy-2,4-dimethyl-6-[1-(toluene-4-sulfonyl)-1H-indol-3-yl]-cyclohexyl}-[1-(toluene-4-sulfonyl)-1H-indol-3-yl]-methanone

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / tetra-n-butylammonium hydrogen sulfate, 50percent aq, KOH / benzene / 0.25 h / Ambient temperature

2: 100 percent / CF₃COOH / 3 h / Ambient temperature

With potassium hydroxide; tetra(n-butyl)ammonium hydrogensulfate; trifluoroacetic acid; In benzene;
DOI:10.1021/jo00249a009

Reference yield:

: 98-59-9
p-toluenesulfonyl chloride

: 114907-12-9
{(1S,2R,6R)-4-Hydroxy-2,4-dimethyl-6-[1-(toluene-4-sulfonyl)-1H-indol-3-yl]-cyclohexyl}-[1-(toluene-4-sulfonyl)-1H-indol-3-yl]-methanone

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / tetra-n-butylammonium hydrogen sulfate, 50percent aq, KOH / benzene / 0.25 h / Ambient temperature

2: 100 percent / CF₃COOH / 3 h / Ambient temperature

With potassium hydroxide; tetra(n-butyl)ammonium hydrogensulfate; trifluoroacetic acid; In benzene;
DOI:10.1021/jo00249a009