methyl [(1R,2S,5R)-(-)-menthoxyacetyl]pyrrolidinium tetrafluoroborate

Base Information

Chemical Name:methyl [(1R,2S,5R)-(-)-menthoxyacetyl]pyrrolidinium tetrafluoroborate
CAS No.:1018348-66-7
Molecular Formula:BF₄*C₁₇H₃₂NO₂
Molecular Weight:369.251
Hs Code.:

Synonyms:methyl [(1R,2S,5R)-(-)-menthoxyacetyl]pyrrolidinium tetrafluoroborate

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Chemical Property of methyl [(1R,2S,5R)-(-)-menthoxyacetyl]pyrrolidinium tetrafluoroborate

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Technology Process of methyl [(1R,2S,5R)-(-)-menthoxyacetyl]pyrrolidinium tetrafluoroborate

There total 2 articles about methyl [(1R,2S,5R)-(-)-menthoxyacetyl]pyrrolidinium tetrafluoroborate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1018332-55-2
methyl [(1R,2S,5R)-(-)-menthoxyacetyl]pyrrolidinium chloride

: 1018348-66-7
methyl [(1R,2S,5R)-(-)-menthoxyacetyl]pyrrolidinium tetrafluoroborate

Guidance literature:: With potassium tetrafluoroborate; In water; at 20 ℃; for 3h;
DOI:10.1016/j.tetlet.2008.01.011

Reference yield:

: 7377-98-2,27994-88-3,88644-14-8,106916-72-7,111957-92-7,21758-29-2
(-)-menthyl chloroacetate

: 1018348-66-7
methyl [(1R,2S,5R)-(-)-menthoxyacetyl]pyrrolidinium tetrafluoroborate

Guidance literature:: Multi-step reaction with 2 steps

1: acetonitrile / 48 h / Inert atmosphere; Reflux

2: tetrafluoroboric acid / water

With tetrafluoroboric acid; In water; acetonitrile;
DOI:10.1016/j.tetlet.2017.01.102