N-[4-(Benzo[b][1,8]phenanthrolin-7-ylamino)-phenyl]-4-methyl-benzenesulfonamide

Base Information

• Chemical Name: N-[4-(Benzo[b][1,8]phenanthrolin-7-ylamino)-phenyl]-4-methyl-benzenesulfonamide
• CAS No.: 132904-26-8
• Molecular Formula: C₂₉H₂₂N₄O₂S
• Molecular Weight: 490.585

Synonyms:N-[4-(Benzo[b][1,8]phenanthrolin-7-ylamino)-phenyl]-4-methyl-benzenesulfonamide

Chemical Property of N-[4-(Benzo[b][1,8]phenanthrolin-7-ylamino)-phenyl]-4-methyl-benzenesulfonamide

Chemical Property:

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Technology Process of N-[4-(Benzo[b][1,8]phenanthrolin-7-ylamino)-phenyl]-4-methyl-benzenesulfonamide

There total 6 articles about N-[4-(Benzo[b][1,8]phenanthrolin-7-ylamino)-phenyl]-4-methyl-benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

N-(4-aminophenyl)-4-methylbenzenesulfonamide (6380-08-1) + 7-chloro-benzo[b][1,8]phenanthroline (97620-83-2) → 12H-benzo<1,8>phenanthrol-7-one (132904-16-6) + N-[4-(Benzo[b][1,8]phenanthrolin-7-ylamino)-phenyl]-4-methyl-benzenesulfonamide (132904-26-8)

Guidance literature:

With methanesulfonic acid; In ethanol; for 0.5h; Heating;

Reference yield:

12H-benzo<1,8>phenanthrol-7-one (132904-16-6) → N-[4-(Benzo[b][1,8]phenanthrolin-7-ylamino)-phenyl]-4-methyl-benzenesulfonamide (132904-26-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 45 percent / PCl₅

2: 55 percent / methanesulfonic acid / ethanol / Heating

With methanesulfonic acid; phosphorus pentachloride; In ethanol;

DOI:10.1002/jps.2600820309

Reference yield:

N-(5-isoquinolyl)anthranilic acid (111880-41-2) → N-[4-(Benzo[b][1,8]phenanthrolin-7-ylamino)-phenyl]-4-methyl-benzenesulfonamide (132904-26-8)

Guidance literature:

Multi-step reaction with 3 steps

1: 60 percent / H₂SO₄ / 5 h / 100 °C

2: 45 percent / PCl₅

3: 55 percent / methanesulfonic acid / ethanol / Heating

With methanesulfonic acid; phosphorus pentachloride; sulfuric acid; In ethanol;

DOI:10.1002/jps.2600820309

upstream raw materials:

N-(4-aminophenyl)-4-methylbenzenesulfonamide

7-chloro-benzo[b][1,8]phenanthroline

12H-benzo<1,8>phenanthrol-7-one

N-(5-isoquinolyl)anthranilic acid

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