methyl 3,7-anhydro-2-deoxy-8-O-trityl-d-gulo-D-glycero-octulonate

Base Information

Chemical Name:methyl 3,7-anhydro-2-deoxy-8-O-trityl-d-gulo-D-glycero-octulonate
CAS No.:603129-42-6
Molecular Formula:C₂₈H₃₀O₇
Molecular Weight:478.542
Hs Code.:

Synonyms:methyl 3,7-anhydro-2-deoxy-8-O-trityl-d-gulo-D-glycero-octulonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 3,7-anhydro-2-deoxy-8-O-trityl-d-gulo-D-glycero-octulonate

Chemical Property:

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Technology Process of methyl 3,7-anhydro-2-deoxy-8-O-trityl-d-gulo-D-glycero-octulonate

There total 3 articles about methyl 3,7-anhydro-2-deoxy-8-O-trityl-d-gulo-D-glycero-octulonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 76-83-5
trityl chloride

: 603129-41-5
((2S,3R,4R,5S,6R)-3,4,5-Trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yl)-acetic acid methyl ester

: 603129-42-6
methyl 3,7-anhydro-2-deoxy-8-O-trityl-d-gulo-D-glycero-octulonate

Guidance literature:: In pyridine; for 16h;
DOI:10.1002/ejoc.200300031

Reference yield:

: 34010-29-2
2-((2S,3S,4R,5R,6R)-3,4,5-triacetoxy-6-(acetoxymethyl)tetrahydro-2H-pyran-2-yl)acetic acid

: 603129-42-6
methyl 3,7-anhydro-2-deoxy-8-O-trityl-d-gulo-D-glycero-octulonate

Guidance literature:: Multi-step reaction with 3 steps

1: 83 percent / DIC; DMAP / CH₂Cl₂ / 3 h / 20 °C

2: NaOMe / methanol / 2 h

3: 85 percent / pyridine / 16 h

With dmap; sodium methylate; dacarbazine; In pyridine; methanol; dichloromethane; 2: Zemplen deacylation;
DOI:10.1002/ejoc.200300031

Reference yield:

: 77838-27-8
methyl 4,5,6,8-tetra-O-acetyl-3,7-anhydro-2-deoxy-D-glycero-D-gulo-octulonate

: 603129-42-6
methyl 3,7-anhydro-2-deoxy-8-O-trityl-d-gulo-D-glycero-octulonate

Guidance literature:: Multi-step reaction with 2 steps

1: NaOMe / methanol / 2 h

2: 85 percent / pyridine / 16 h

With sodium methylate; In pyridine; methanol; 1: Zemplen deacylation;
DOI:10.1002/ejoc.200300031