2,3-bis-dimethylamino-1,4-bis-(2,6-dimethyl-phenyl)-3,4-dihydro-2H-[1,4,2,3]diazadiborol-1-ium; trifluoro-methanesulfonate

Base Information

Chemical Name:2,3-bis-dimethylamino-1,4-bis-(2,6-dimethyl-phenyl)-3,4-dihydro-2H-[1,4,2,3]diazadiborol-1-ium; trifluoro-methanesulfonate
CAS No.:850816-21-6
Molecular Formula:CF₃O₃S*C₂₁H₃₁B₂N₄
Molecular Weight:510.196
Hs Code.:

2,3-bis-dimethylamino-1,4-bis-(2,6-dimethyl-phenyl)-3,4-dihydro-2<i>H</i>-[1,4,2,3]diazadiborol-1-ium; trifluoro-methanesulfonate

Synonyms:2,3-bis-dimethylamino-1,4-bis-(2,6-dimethyl-phenyl)-3,4-dihydro-2H-[1,4,2,3]diazadiborol-1-ium; trifluoro-methanesulfonate

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Chemical Property of 2,3-bis-dimethylamino-1,4-bis-(2,6-dimethyl-phenyl)-3,4-dihydro-2H-[1,4,2,3]diazadiborol-1-ium; trifluoro-methanesulfonate

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Technology Process of 2,3-bis-dimethylamino-1,4-bis-(2,6-dimethyl-phenyl)-3,4-dihydro-2H-[1,4,2,3]diazadiborol-1-ium; trifluoro-methanesulfonate

There total 4 articles about 2,3-bis-dimethylamino-1,4-bis-(2,6-dimethyl-phenyl)-3,4-dihydro-2H-[1,4,2,3]diazadiborol-1-ium; trifluoro-methanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: C₂₀H₂₈N₂Si

: 64541-76-0
dichlorobis(dimethylamino)diborane⁽⁴⁾

: 27607-77-8
trimethylsilyl trifluoromethanesulfonate

: 850816-21-6
2,3-bis-dimethylamino-1,4-bis-(2,6-dimethyl-phenyl)-3,4-dihydro-2H-[1,4,2,3]diazadiborol-1-ium; trifluoro-methanesulfonate

Guidance literature:: C₂₀H₂₈N₂Si; dichlorobis(dimethylamino)diborane⁽⁴⁾; In dichloromethane; at 20 ℃; for 1h;

trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at 20 ℃; for 1h;
DOI:10.1021/ja050129e

Reference yield:

: 87-62-7
2,6-dimethylaniline

: 850816-21-6
2,3-bis-dimethylamino-1,4-bis-(2,6-dimethyl-phenyl)-3,4-dihydro-2H-[1,4,2,3]diazadiborol-1-ium; trifluoro-methanesulfonate

Guidance literature:: Multi-step reaction with 3 steps

1.1: 52 percent / AcOH / 160 °C

2.1: n-BuLi / hexane; tetrahydrofuran / 2 h

2.2: 91 percent / tetrahydrofuran; hexane

3.1: CH₂Cl₂ / 1 h / 20 °C

3.2: 94 percent / CH₂Cl₂ / 1 h / 20 °C

With n-butyllithium; acetic acid; In tetrahydrofuran; hexane; dichloromethane;
DOI:10.1021/ja050129e

Reference yield:

: 16596-05-7
(E)-N,N'-bis(2,6-dimethylphenyl)formimidamide

: 850816-21-6
2,3-bis-dimethylamino-1,4-bis-(2,6-dimethyl-phenyl)-3,4-dihydro-2H-[1,4,2,3]diazadiborol-1-ium; trifluoro-methanesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-BuLi / hexane; tetrahydrofuran / 2 h

1.2: 91 percent / tetrahydrofuran; hexane

2.1: CH₂Cl₂ / 1 h / 20 °C

2.2: 94 percent / CH₂Cl₂ / 1 h / 20 °C

With n-butyllithium; In tetrahydrofuran; hexane; dichloromethane;
DOI:10.1021/ja050129e