9-(2,4,6-tri-O-acetyl-3-deoxy-3-fluoro-β-D-glucopyranosyl)-N⁶-benzoyl adenine

Base Information

• Chemical Name: 9-(2,4,6-tri-O-acetyl-3-deoxy-3-fluoro-β-D-glucopyranosyl)-N⁶-benzoyl adenine
• CAS No.: 1020068-54-5
• Molecular Formula: C₂₄H₂₄FN₅O₈
• Molecular Weight: 529.482

Synonyms:9-(2,4,6-tri-O-acetyl-3-deoxy-3-fluoro-β-D-glucopyranosyl)-N⁶-benzoyl adenine

Chemical Property of 9-(2,4,6-tri-O-acetyl-3-deoxy-3-fluoro-β-D-glucopyranosyl)-N⁶-benzoyl adenine

Chemical Property:

Purity/Quality:

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Technology Process of 9-(2,4,6-tri-O-acetyl-3-deoxy-3-fluoro-β-D-glucopyranosyl)-N⁶-benzoyl adenine

There total 1 articles about 9-(2,4,6-tri-O-acetyl-3-deoxy-3-fluoro-β-D-glucopyranosyl)-N⁶-benzoyl adenine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

[(2R,3R,4S,5S)-3,5,6-triacetoxy-4-fluoro-tetrahydropyran-2-yl]methyl acetate (7226-43-9,20409-32-9,22434-91-9,22434-92-0,88198-26-9,83602-93-1) + N-benzoyladenine (4005-49-6) → 9-(2,4,6-tri-O-acetyl-3-deoxy-3-fluoro-β-D-glucopyranosyl)-N6-benzoyl adenine (1020068-54-5)

Guidance literature:

N-benzoyladenine; With 1,1,1,3,3,3-hexamethyl-disilazane; saccharin; In acetonitrile; at 120 ℃; for 0.5h;

[(2R,3R,4S,5S)-3,5,6-triacetoxy-4-fluoro-tetrahydropyran-2-yl]methyl acetate; With tin chloride; In acetonitrile; at 100 ℃; for 5h; Further stages.;

DOI:10.1016/j.ejmech.2007.04.001

Reference yield: 88.0%

9-(2,4,6-tri-O-acetyl-3-deoxy-3-fluoro-β-D-glucopyranosyl)-N6-benzoyl adenine (1020068-54-5) → 9-(3-deoxy-3-fluoro-β-D-glucopyranosyl)-N6-benzoyl adenine (1020068-55-6)

Guidance literature:

With pyridine; sodium hydroxide; In ethanol; at 0 ℃; for 0.5h;

DOI:10.1016/j.ejmech.2007.04.001

upstream raw materials:

[(2R,3R,4S,5S)-3,5,6-triacetoxy-4-fluoro-tetrahydropyran-2-yl]methyl acetate

N-benzoyladenine

Downstream raw materials:

9-(3-deoxy-3-fluoro-β-D-glucopyranosyl)-N⁶-benzoyl adenine

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