DL-(1α,2α,4α,5α,7α,8α)-6-(4-Methylphenylsulfonyl)-3-oxa-6-azatetracyclo<6.1.0.0^2,4.0^5,7>nonan

Base Information

• Chemical Name: DL-(1α,2α,4α,5α,7α,8α)-6-(4-Methylphenylsulfonyl)-3-oxa-6-azatetracyclo<6.1.0.0^2,4.0^5,7>nonan
• CAS No.: 112297-70-8
• Molecular Formula: C₁₄H₁₅NO₃S
• Molecular Weight: 277.344

Synonyms:DL-(1α,2α,4α,5α,7α,8α)-6-(4-Methylphenylsulfonyl)-3-oxa-6-azatetracyclo<6.1.0.0^2,4.0^5,7>nonan

Chemical Property of DL-(1α,2α,4α,5α,7α,8α)-6-(4-Methylphenylsulfonyl)-3-oxa-6-azatetracyclo<6.1.0.0^2,4.0^5,7>nonan

Chemical Property:

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Technology Process of DL-(1α,2α,4α,5α,7α,8α)-6-(4-Methylphenylsulfonyl)-3-oxa-6-azatetracyclo<6.1.0.0^2,4.0^5,7>nonan

There total 1 articles about DL-(1α,2α,4α,5α,7α,8α)-6-(4-Methylphenylsulfonyl)-3-oxa-6-azatetracyclo<6.1.0.0^2,4.0^5,7>nonan which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

diazomethane (186581-53-3,908094-01-9,334-88-3) + DL-(1α,2α,4α,7α)-8-(4-Methylphenylsulfonyl)-3-oxa-8-azatricyclo<5.1.0.02,4>oct-5-en (112419-21-3) → DL-(1α,2β,4β,5β,7β,8α)-6-(4-Methylphenylsulfonyl)-3-oxa-6-azatetracyclo<6.1.0.02,4.05,7>nonan (112419-24-6) + DL-(1α,2α,4α,5α,7α,8α)-6-(4-Methylphenylsulfonyl)-3-oxa-6-azatetracyclo<6.1.0.02,4.05,7>nonan (112297-70-8)

Guidance literature:

Yield given. Multistep reaction. Yields of byproduct given; 1.) ether, CHCl₂, 8 d, 5 deg C; 2.) acetone, 80 min, -20 deg C, irradiation;

Reference yield: 82.0%

DL-(1α,2α,4α,5α,7α,8α)-6-(4-Methylphenylsulfonyl)-3-oxa-6-azatetracyclo<6.1.0.02,4.05,7>nonan (112297-70-8) → DL-(Z,Z,Z)-4,7-Dihydro-4-(4-methylphenylsulfonyl)-1,4-oxazonin (112297-75-3)

Guidance literature:

With iodine; In chloroform; for 72h; Ambient temperature;

upstream raw materials:

diazomethane

DL-(1α,2α,4α,7α)-8-(4-Methylphenylsulfonyl)-3-oxa-8-azatricyclo<5.1.0.0^2,4>oct-5-en

Downstream raw materials:

DL-(Z,Z,Z)-4,7-Dihydro-4-(4-methylphenylsulfonyl)-1,4-oxazonin

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