C₆₂H₉₆O₁₁Si₂

Base Information

• Chemical Name: C₆₂H₉₆O₁₁Si₂
• CAS No.: 1360873-01-3
• Molecular Formula: C₆₂H₉₆O₁₁Si₂
• Molecular Weight: 1073.61
• Mol file: 1360873-01-3.mol

Synonyms:C₆₂H₉₆O₁₁Si₂

Chemical Property of C₆₂H₉₆O₁₁Si₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₆₂H₉₆O₁₁Si₂

There total 1 articles about C₆₂H₉₆O₁₁Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

C48H65O8PSi2 (1028432-58-7) + C26H40O7 (1360872-79-2) → C62H96O11Si2 (1360873-01-3)

Guidance literature:

C₂₆H₄₀O₇; With 9-bora-bicyclo[3.3.1]nonane; In tetrahydrofuran; at 20 ℃; for 1.5h;

With caesium carbonate; In tetrahydrofuran; water; at 20 ℃; for 0.333333h;

C₄₈H₆₅O₈PSi₂; With tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; water; N,N-dimethyl-formamide; at 50 ℃;

DOI:10.1002/chem.201101437

Reference yield: 93.0%

C62H96O11Si2 (1360873-01-3) → C62H98O12Si2 (1360873-10-4)

Guidance literature:

C₆₂H₉₆O₁₁Si₂; With dimethylsulfide borane complex; In tetrahydrofuran; at 0 - 20 ℃;

With dihydrogen peroxide; sodium hydroxide; In tetrahydrofuran; water; at 0 - 20 ℃; optical yield given as %de; stereoselective reaction;

DOI:10.1002/chem.201101437

Reference yield:

C62H96O11Si2 (1360873-01-3) → C38H60O9S (1028433-12-6)

Guidance literature:

Multi-step reaction with 3 steps

1.1: dimethylsulfide borane complex / tetrahydrofuran / 0 - 20 °C

1.2: 0 - 20 °C

2.1: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 0 - 20 °C / Molecular sieve

3.1: hydrogenchloride / tetrahydrofuran; methanol; water / 21.5 h / 60 °C

3.2: 20 h / 20 °C

With hydrogenchloride; tetrapropylammonium perruthennate; dimethylsulfide borane complex; 4-methylmorpholine N-oxide; In tetrahydrofuran; methanol; dichloromethane; water;

DOI:10.1002/chem.201101437

upstream raw materials:

C₄₈H₆₅O₈PSi₂

C₂₆H₄₀O₇

Downstream raw materials:

C₃₆H₅₆O₁₀

C₃₆H₅₆O₁₀

C₃₈H₆₀O₉S

C₅₆H₁₀₂O₉SSi₃