Dimethyl 5'-oxo-7'-(((6-(tritylthio)hexyl)oxy)carbamoyl)-1',5'-dihydrospiro[[1,3]dioxolane-2,4'-pyrrolo[2,3-f]quinoline]-2',9'-dicarboxylate

Base Information

Chemical Name:Dimethyl 5'-oxo-7'-(((6-(tritylthio)hexyl)oxy)carbamoyl)-1',5'-dihydrospiro[[1,3]dioxolane-2,4'-pyrrolo[2,3-f]quinoline]-2',9'-dicarboxylate
CAS No.:1312296-47-1
Molecular Formula:C₄₃H₄₁N₃O₉S
Molecular Weight:775.879
Hs Code.:

Synonyms:Dimethyl 5'-oxo-7'-(((6-(tritylthio)hexyl)oxy)carbamoyl)-1',5'-dihydrospiro[[1,3]dioxolane-2,4'-pyrrolo[2,3-f]quinoline]-2',9'-dicarboxylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Dimethyl 5'-oxo-7'-(((6-(tritylthio)hexyl)oxy)carbamoyl)-1',5'-dihydrospiro[[1,3]dioxolane-2,4'-pyrrolo[2,3-f]quinoline]-2',9'-dicarboxylate

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of Dimethyl 5'-oxo-7'-(((6-(tritylthio)hexyl)oxy)carbamoyl)-1',5'-dihydrospiro[[1,3]dioxolane-2,4'-pyrrolo[2,3-f]quinoline]-2',9'-dicarboxylate

There total 3 articles about Dimethyl 5'-oxo-7'-(((6-(tritylthio)hexyl)oxy)carbamoyl)-1',5'-dihydrospiro[[1,3]dioxolane-2,4'-pyrrolo[2,3-f]quinoline]-2',9'-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: O-(6-(tritylthio)hexyl)hydroxylamine

: 1312296-42-6
2',9'-bis(methoxycarbonyl)-5'-oxo-1',5'-dihydrospiro[[1,3]dioxolane-2,4'-pyrrolo[2,3-f]quinoline]-7'-carboxylic acid pyridine salt

: 1312296-47-1
Dimethyl 5'-oxo-7'-(((6-(tritylthio)hexyl)oxy)carbamoyl)-1',5'-dihydrospiro[[1,3]dioxolane-2,4'-pyrrolo[2,3-f]quinoline]-2',9'-dicarboxylate

Guidance literature:: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃; for 90h; Inert atmosphere;

Reference yield:

: 74447-88-4
trimethyl 4,5-dihydro-4,5-dioxo-1H-pyrrolo[2,3-f]quinoline-2,7,9-tricarboxylate

: 1312296-47-1
Dimethyl 5'-oxo-7'-(((6-(tritylthio)hexyl)oxy)carbamoyl)-1',5'-dihydrospiro[[1,3]dioxolane-2,4'-pyrrolo[2,3-f]quinoline]-2',9'-dicarboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: toluene-4-sulfonic acid / benzene / 14 h / Reflux

2: water / 120 h / 20 °C

3: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / dichloromethane / 90 h / 20 °C / Inert atmosphere

With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; toluene-4-sulfonic acid; In dichloromethane; water; benzene;

Reference yield:

: 1312296-40-4
Trimethyl 5'-oxo-1',5'-dihydrospiro[[1,3]dioxolane-2,4'-pyrrolo[2,3-f]quinoline]-2',7',9'-tricarboxylate

: 1312296-47-1
Dimethyl 5'-oxo-7'-(((6-(tritylthio)hexyl)oxy)carbamoyl)-1',5'-dihydrospiro[[1,3]dioxolane-2,4'-pyrrolo[2,3-f]quinoline]-2',9'-dicarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: water / 120 h / 20 °C

2: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / dichloromethane / 90 h / 20 °C / Inert atmosphere

With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; water;