C₂₉H₃₀O₉S₂

Base Information

• Chemical Name: C₂₉H₃₀O₉S₂
• CAS No.: 1180502-80-0
• Molecular Formula: C₂₉H₃₀O₉S₂
• Molecular Weight: 586.684
• Mol file: 1180502-80-0.mol

Synonyms:C₂₉H₃₀O₉S₂

Chemical Property of C₂₉H₃₀O₉S₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₉H₃₀O₉S₂

There total 8 articles about C₂₉H₃₀O₉S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C19H22O6 → C29H30O9S2 (1180502-80-0)

Guidance literature:

Multi-step reaction with 7 steps

1: pyridine; dmap / 16 h / 20 °C

2: hydrogenchloride / dichloromethane / 17 h / 0 - 15 °C / Sealed tube

3: 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride / toluene / 2 h / Heating

4: ammonia / methanol / 16 h / 20 °C / Sealed tube

5: camphorsulphonic acid / N,N-dimethyl-formamide / 4 h / 55 °C

6: 2,3-dicyano-5,6-dichloro-p-benzoquinone; water / dichloromethane / 16 h

7: pyridine / 96 h

With pyridine; hydrogenchloride; dmap; 2,2'-azobis(isobutyronitrile); ammonia; water; tri-n-butyl-tin hydride; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In methanol; dichloromethane; N,N-dimethyl-formamide; toluene;

DOI:10.1021/ol401730d

Reference yield:

benzaldehyde dimethyl acetal (1125-88-8) → C29H30O9S2 (1180502-80-0)

Guidance literature:

Multi-step reaction with 3 steps

1: camphorsulphonic acid / N,N-dimethyl-formamide / 4 h / 55 °C

2: 2,3-dicyano-5,6-dichloro-p-benzoquinone; water / dichloromethane / 16 h

3: pyridine / 96 h

With pyridine; water; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; N,N-dimethyl-formamide;

DOI:10.1021/ol401730d

Reference yield:

C27H30O10 (1449674-08-1) → C29H30O9S2 (1180502-80-0)

Guidance literature:

Multi-step reaction with 6 steps

1: hydrogenchloride / dichloromethane / 17 h / 0 - 15 °C / Sealed tube

2: 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride / toluene / 2 h / Heating

3: ammonia / methanol / 16 h / 20 °C / Sealed tube

4: camphorsulphonic acid / N,N-dimethyl-formamide / 4 h / 55 °C

5: 2,3-dicyano-5,6-dichloro-p-benzoquinone; water / dichloromethane / 16 h

6: pyridine / 96 h

With pyridine; hydrogenchloride; 2,2'-azobis(isobutyronitrile); ammonia; water; tri-n-butyl-tin hydride; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In methanol; dichloromethane; N,N-dimethyl-formamide; toluene;

DOI:10.1021/ol401730d

upstream raw materials:

C₂₇H₃₀O₁₀

benzaldehyde dimethyl acetal

C₂₅H₂₈O₈

C₁₉H₂₂O₅

Downstream raw materials:

C₂₂H₂₄O₇S

C₁₅H₁₆O₄

C₁₄H₁₆O₅

C₁₈H₂₀N₂O₇