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Technology Process of N2-{2-[1,3-dihydro-2H-isoindol-2-yl(methyl)amino]-2-oxoethyl}-N2-{4-[4-(methoxycarbonyl)-2-oxopyrrolidin-1-yl]-2-methylphenyl}-N1-{2-[(tert-butoxycarbonyl)(ethyl)amino]ethyl}glycinamide

N2-{2-[1,3-dihydro-2H-isoindol-2-yl(methyl)amino]-2-oxoethyl}-N2-{4-[4-(methoxycarbonyl)-2-oxopyrrolidin-1-yl]-2-methylphenyl}-N1-{2-[(tert-butoxycarbonyl)(ethyl)amino]ethyl}glycinamide

Base Information
  • Chemical Name:N2-{2-[1,3-dihydro-2H-isoindol-2-yl(methyl)amino]-2-oxoethyl}-N2-{4-[4-(methoxycarbonyl)-2-oxopyrrolidin-1-yl]-2-methylphenyl}-N1-{2-[(tert-butoxycarbonyl)(ethyl)amino]ethyl}glycinamide
  • CAS No.:1190896-98-0
  • Molecular Formula:C35H48N6O7
  • Molecular Weight:664.802
  • Hs Code.:
N<sub>2</sub>-{2-[1,3-dihydro-2H-isoindol-2-yl(methyl)amino]-2-oxoethyl}-N<sub>2</sub>-{4-[4-(methoxycarbonyl)-2-oxopyrrolidin-1-yl]-2-methylphenyl}-N<sub>1</sub>-{2-[(tert-butoxycarbonyl)(ethyl)amino]ethyl}glycinamide

Synonyms:N2-{2-[1,3-dihydro-2H-isoindol-2-yl(methyl)amino]-2-oxoethyl}-N2-{4-[4-(methoxycarbonyl)-2-oxopyrrolidin-1-yl]-2-methylphenyl}-N1-{2-[(tert-butoxycarbonyl)(ethyl)amino]ethyl}glycinamide

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Chemical Property of N2-{2-[1,3-dihydro-2H-isoindol-2-yl(methyl)amino]-2-oxoethyl}-N2-{4-[4-(methoxycarbonyl)-2-oxopyrrolidin-1-yl]-2-methylphenyl}-N1-{2-[(tert-butoxycarbonyl)(ethyl)amino]ethyl}glycinamide
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Technology Process of N2-{2-[1,3-dihydro-2H-isoindol-2-yl(methyl)amino]-2-oxoethyl}-N2-{4-[4-(methoxycarbonyl)-2-oxopyrrolidin-1-yl]-2-methylphenyl}-N1-{2-[(tert-butoxycarbonyl)(ethyl)amino]ethyl}glycinamide

There total 1 articles about N2-{2-[1,3-dihydro-2H-isoindol-2-yl(methyl)amino]-2-oxoethyl}-N2-{4-[4-(methoxycarbonyl)-2-oxopyrrolidin-1-yl]-2-methylphenyl}-N1-{2-[(tert-butoxycarbonyl)(ethyl)amino]ethyl}glycinamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

N<sub>2</sub>-{2-[1,3-dihydro-2H-isoindol-2-yl(methyl)amino]-2-oxoethyl}-N<sub>2</sub>-(4-iodo-2-methylphenyl)-N<sub>1</sub>-{2-[(tert-butoxycarbonyl)(ethyl)amino]ethyl}glycinamide
1190896-92-4

N2-{2-[1,3-dihydro-2H-isoindol-2-yl(methyl)amino]-2-oxoethyl}-N2-(4-iodo-2-methylphenyl)-N1-{2-[(tert-butoxycarbonyl)(ethyl)amino]ethyl}glycinamide

5-oxopyrrolidine-3-carboxylic acid methyl ester
35309-35-4,428518-31-4

5-oxopyrrolidine-3-carboxylic acid methyl ester

N<sub>2</sub>-{2-[1,3-dihydro-2H-isoindol-2-yl(methyl)amino]-2-oxoethyl}-N<sub>2</sub>-{4-[4-(methoxycarbonyl)-2-oxopyrrolidin-1-yl]-2-methylphenyl}-N<sub>1</sub>-{2-[(tert-butoxycarbonyl)(ethyl)amino]ethyl}glycinamide
1190896-98-0

N2-{2-[1,3-dihydro-2H-isoindol-2-yl(methyl)amino]-2-oxoethyl}-N2-{4-[4-(methoxycarbonyl)-2-oxopyrrolidin-1-yl]-2-methylphenyl}-N1-{2-[(tert-butoxycarbonyl)(ethyl)amino]ethyl}glycinamide

Guidance literature:

Reference yield:

1-hydroxy-7-aza-benzotriazole
39968-33-7

1-hydroxy-7-aza-benzotriazole

N<sub>2</sub>-{2-[1,3-dihydro-2H-isoindol-2-yl(methyl)amino]-2-oxoethyl}-N<sub>2</sub>-{4-[4-(methoxycarbonyl)-2-oxopyrrolidin-1-yl]-2-methylphenyl}-N<sub>1</sub>-{2-[(tert-butoxycarbonyl)(ethyl)amino]ethyl}glycinamide
1190896-98-0

N2-{2-[1,3-dihydro-2H-isoindol-2-yl(methyl)amino]-2-oxoethyl}-N2-{4-[4-(methoxycarbonyl)-2-oxopyrrolidin-1-yl]-2-methylphenyl}-N1-{2-[(tert-butoxycarbonyl)(ethyl)amino]ethyl}glycinamide

citric acid
77-92-9,906507-37-7

citric acid

N<sub>2</sub>-{4-[4-(aminocarbonyl)-2-oxopyrrolidin-1-yl]-2-methylphenyl}-N<sub>2</sub>-{2-[1,3-dihydro-2H-isoindol-2-yl(methyl)amino]-2-oxoethyl}-N<sub>1</sub>-{2-[(tert-butoxycarbonyl)(ethyl)amino]ethyl}glycinamide
1190896-99-1

N2-{4-[4-(aminocarbonyl)-2-oxopyrrolidin-1-yl]-2-methylphenyl}-N2-{2-[1,3-dihydro-2H-isoindol-2-yl(methyl)amino]-2-oxoethyl}-N1-{2-[(tert-butoxycarbonyl)(ethyl)amino]ethyl}glycinamide

Guidance literature:
With aqueous ammonia; aqueous sodium hydroxide; In methanol; N,N-dimethyl-formamide;
upstream raw materials:

N2-{2-[1,3-dihydro-2H-isoindol-2-yl(methyl)amino]-2-oxoethyl}-N2-(4-iodo-2-methylphenyl)-N1-{2-[(tert-butoxycarbonyl)(ethyl)amino]ethyl}glycinamide

5-oxopyrrolidine-3-carboxylic acid methyl ester

Downstream raw materials:

N2-{4-[4-(aminocarbonyl)-2-oxopyrrolidin-1-yl]-2-methylphenyl}-N2-{2-[1,3-dihydro-2H-isoindol-2-yl(methyl)amino]-2-oxoethyl}-N1-{2-[(tert-butoxycarbonyl)(ethyl)amino]ethyl}glycinamide

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