N,N'-[cyclohexane-1,1-diylbis(oxyethane-2,1-diyl)]bis(2,2,2-trifluoroacetamide)

Base Information

Chemical Name:N,N'-[cyclohexane-1,1-diylbis(oxyethane-2,1-diyl)]bis(2,2,2-trifluoroacetamide)
CAS No.:1415392-94-7
Molecular Formula:C₁₄H₂₀F₆N₂O₄
Molecular Weight:394.314
Hs Code.:

Synonyms:N,N'-[cyclohexane-1,1-diylbis(oxyethane-2,1-diyl)]bis(2,2,2-trifluoroacetamide)

Suppliers and Price of N,N'-[cyclohexane-1,1-diylbis(oxyethane-2,1-diyl)]bis(2,2,2-trifluoroacetamide)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N,N'-[cyclohexane-1,1-diylbis(oxyethane-2,1-diyl)]bis(2,2,2-trifluoroacetamide)

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Technology Process of N,N'-[cyclohexane-1,1-diylbis(oxyethane-2,1-diyl)]bis(2,2,2-trifluoroacetamide)

There total 2 articles about N,N'-[cyclohexane-1,1-diylbis(oxyethane-2,1-diyl)]bis(2,2,2-trifluoroacetamide) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 6974-29-4
N-(2-hydroxyethyl)-2,2,2-trifluoroacetamide

: 1122-84-5
1-ethoxycyclohexene

: 1670-47-9
1,1-diethoxycyclohexane

: 1415392-94-7
N,N'-[cyclohexane-1,1-diylbis(oxyethane-2,1-diyl)]bis(2,2,2-trifluoroacetamide)

Guidance literature:: With hydrogenchloride; In diethyl ether; for 3 - 11h; Reflux;
DOI:10.1134/S1070428012100053

Reference yield: 43.0%

: 6974-29-4
N-(2-hydroxyethyl)-2,2,2-trifluoroacetamide

: 108-94-1,11119-77-0,9003-41-2,9075-99-4
cyclohexanone

: 1415392-94-7
N,N'-[cyclohexane-1,1-diylbis(oxyethane-2,1-diyl)]bis(2,2,2-trifluoroacetamide)

Guidance literature:: N-(2-hydroxyethyl)-2,2,2-trifluoroacetamide; cyclohexanone; With toluene-4-sulfonic acid; In tetrahydrofuran; for 0.5h; Molecular sieve; Inert atmosphere;

With sulfuric acid; In tetrahydrofuran; at 20 ℃; Molecular sieve; Inert atmosphere;
DOI:10.1021/jacs.6b11181