N,N'-Bis(p-tolylsulfonyl)-N,N'-bis<8-(p-tolylsulfonyloxy)octanyl>-4,4'-diaminodiphenylmethane

Base Information

Chemical Name:N,N'-Bis(p-tolylsulfonyl)-N,N'-bis<8-(p-tolylsulfonyloxy)octanyl>-4,4'-diaminodiphenylmethane
CAS No.:129687-98-5
Molecular Formula:C₅₇H₇₀N₂O₁₀S₄
Molecular Weight:1071.45
Hs Code.:

Synonyms:N,N'-Bis(p-tolylsulfonyl)-N,N'-bis<8-(p-tolylsulfonyloxy)octanyl>-4,4'-diaminodiphenylmethane

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Chemical Property of N,N'-Bis(p-tolylsulfonyl)-N,N'-bis<8-(p-tolylsulfonyloxy)octanyl>-4,4'-diaminodiphenylmethane

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Technology Process of N,N'-Bis(p-tolylsulfonyl)-N,N'-bis<8-(p-tolylsulfonyloxy)octanyl>-4,4'-diaminodiphenylmethane

There total 4 articles about N,N'-Bis(p-tolylsulfonyl)-N,N'-bis<8-(p-tolylsulfonyloxy)octanyl>-4,4'-diaminodiphenylmethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 129687-97-4
N,N'-bis(p-tolylsulfonyl)-N,N'-bis(8-hydroxyoctanyl)-4,4'-diaminodiphenylmethane

: 98-59-9
p-toluenesulfonyl chloride

: 129687-98-5
N,N'-Bis(p-tolylsulfonyl)-N,N'-bis<8-(p-tolylsulfonyloxy)octanyl>-4,4'-diaminodiphenylmethane

Guidance literature:: With dmap; triethylamine; In dichloromethane; for 0.5h; Ambient temperature;

Reference yield:

: 50816-20-1
2-(8-bromooctyloxy)tetrahydropyran

: 129687-98-5
N,N'-Bis(p-tolylsulfonyl)-N,N'-bis<8-(p-tolylsulfonyloxy)octanyl>-4,4'-diaminodiphenylmethane

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / K₂CO₃ / dimethylformamide / 5 h / 120 °C

2: 95 percent / p-TsOH / methanol / 0.67 h / Ambient temperature

3: 90 percent / NEt₃, DMAP / CH₂Cl₂ / 0.5 h / Ambient temperature

With dmap; potassium carbonate; toluene-4-sulfonic acid; triethylamine; In methanol; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 74043-79-1
4,4’-methylenebis(N-p-tosylanilide)

: 129687-98-5
N,N'-Bis(p-tolylsulfonyl)-N,N'-bis<8-(p-tolylsulfonyloxy)octanyl>-4,4'-diaminodiphenylmethane

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / K₂CO₃ / dimethylformamide / 5 h / 120 °C

2: 95 percent / p-TsOH / methanol / 0.67 h / Ambient temperature

3: 90 percent / NEt₃, DMAP / CH₂Cl₂ / 0.5 h / Ambient temperature

With dmap; potassium carbonate; toluene-4-sulfonic acid; triethylamine; In methanol; dichloromethane; N,N-dimethyl-formamide;