(2-((4-pentylphenyl)ethynyl)phenyl)methanol

Base Information

• Chemical Name: (2-((4-pentylphenyl)ethynyl)phenyl)methanol
• CAS No.: 1620151-49-6
• Molecular Formula: C₂₀H₂₂O
• Molecular Weight: 278.394
• Mol file: 1620151-49-6.mol

Synonyms:(2-((4-pentylphenyl)ethynyl)phenyl)methanol

Chemical Property of (2-((4-pentylphenyl)ethynyl)phenyl)methanol

Chemical Property:

Purity/Quality:

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Technology Process of (2-((4-pentylphenyl)ethynyl)phenyl)methanol

There total 1 articles about (2-((4-pentylphenyl)ethynyl)phenyl)methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-iodobenzyl alcohol (5159-41-1) + 1-ethynyl-4-(n-pentyl)benzene (79887-10-8) → (2-((4-pentylphenyl)ethynyl)phenyl)methanol (1620151-49-6)

Guidance literature:

With piperidine; bis-triphenylphosphine-palladium(II) chloride; at 70 ℃; for 12h; Inert atmosphere;

DOI:10.1002/ejoc.201402611

Reference yield: 45.0%

(2-((4-pentylphenyl)ethynyl)phenyl)methanol (1620151-49-6) + N’-(2-hydroxybenzylidene)-4-methylbenzene-1-sulfonohydrazide (1666-14-4) → 6a-(4-pentylphenyl)-5,6a-dihydroisochromeno[3,4-b]chromene (1620151-62-3)

Guidance literature:

With copper(II) perchlorate hexahydrate; In 1,4-dioxane; toluene; at 60 ℃; for 11h; Inert atmosphere;

DOI:10.1039/c4cc02862g

Reference yield:

(2-((4-pentylphenyl)ethynyl)phenyl)methanol (1620151-49-6) → C20H21Br

Guidance literature:

With pyridine; phosphorus tribromide; In chloroform; at 0 - 20 ℃; for 13h;

DOI:10.1002/ejoc.201402611

upstream raw materials:

2-iodobenzyl alcohol

1-ethynyl-4-(n-pentyl)benzene

Downstream raw materials:

6a-(4-pentylphenyl)-5,6a-dihydroisochromeno[3,4-b]chromene