propyl 5-iodo-2-((8-(2-methyl-1,3-dioxolan-2-yl)oct-2-yn-1-yl)oxy)benzoate

Base Information

Chemical Name:propyl 5-iodo-2-((8-(2-methyl-1,3-dioxolan-2-yl)oct-2-yn-1-yl)oxy)benzoate
CAS No.:1505448-07-6
Molecular Formula:C₂₂H₂₉IO₅
Molecular Weight:500.374
Hs Code.:

Synonyms:propyl 5-iodo-2-((8-(2-methyl-1,3-dioxolan-2-yl)oct-2-yn-1-yl)oxy)benzoate

Suppliers and Price of propyl 5-iodo-2-((8-(2-methyl-1,3-dioxolan-2-yl)oct-2-yn-1-yl)oxy)benzoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of propyl 5-iodo-2-((8-(2-methyl-1,3-dioxolan-2-yl)oct-2-yn-1-yl)oxy)benzoate

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Technology Process of propyl 5-iodo-2-((8-(2-methyl-1,3-dioxolan-2-yl)oct-2-yn-1-yl)oxy)benzoate

There total 4 articles about propyl 5-iodo-2-((8-(2-methyl-1,3-dioxolan-2-yl)oct-2-yn-1-yl)oxy)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1505447-79-9
8-(2-methyl-1,3-dioxolan-2-yl)oct-2-yn-1-yl methanesulfonate

: 15125-86-7
2-Hydroxy-5-iodo-benzoic acid propyl ester

: 1505448-07-6
propyl 5-iodo-2-((8-(2-methyl-1,3-dioxolan-2-yl)oct-2-yn-1-yl)oxy)benzoate

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 12h;
DOI:10.1021/ol4031638

Reference yield:

: 1373351-18-8
8-(2-methyl-1,3-dioxolan-2-yl)oct-2-yn-1-ol

: 1505448-07-6
propyl 5-iodo-2-((8-(2-methyl-1,3-dioxolan-2-yl)oct-2-yn-1-yl)oxy)benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 0 °C

2: potassium carbonate / N,N-dimethyl-formamide / 12 h / 20 °C

With potassium carbonate; triethylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ol4031638

Reference yield:

: C₁₈H₃₄O₃Si

: 1505448-07-6
propyl 5-iodo-2-((8-(2-methyl-1,3-dioxolan-2-yl)oct-2-yn-1-yl)oxy)benzoate

Guidance literature:: Multi-step reaction with 3 steps

1: tetrabutyl ammonium fluoride / tetrahydrofuran / 20 °C

2: triethylamine / dichloromethane / 0 °C

3: potassium carbonate / N,N-dimethyl-formamide / 12 h / 20 °C

With tetrabutyl ammonium fluoride; potassium carbonate; triethylamine; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ol4031638